ChemicalBook > CAS DataBase List > 2-IODOBENZOTHIAZOLE

2-IODOBENZOTHIAZOLE

Product Name
2-IODOBENZOTHIAZOLE
CAS No.
1123-99-5
Chemical Name
2-IODOBENZOTHIAZOLE
Synonyms
2-IODOBENZOTHIAZOLE;Benzothiazole, 2-iodo-;2-Iodobenzo[d]thiazole;2-iodo-1,3-benzothiazole
CBNumber
CB12446562
Molecular Formula
C7H4INS
Formula Weight
261.08
MOL File
1123-99-5.mol
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2-IODOBENZOTHIAZOLE Property

Melting point:
77.0 to 81.0 °C
Boiling point:
318.3±25.0 °C(Predicted)
Density 
2.034±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
soluble in Methanol
form 
powder to crystal
pka
0.01±0.10(Predicted)
color 
White to Light yellow to Light orange
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Safety

HS Code 
2934208090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
I0938
Product name
2-Iodobenzothiazole
Purity
>98.0%(GC)
Packaging
1g
Price
$111
Updated
2025/07/31
TCI Chemical
Product number
I0938
Product name
2-Iodobenzothiazole
Purity
>98.0%(GC)
Packaging
5g
Price
$334
Updated
2025/07/31
TRC
Product number
I737103
Product name
2-Iodobenzo[d]thiazole
Packaging
50mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
X9008
Product name
2-Iodobenzothiazole
Packaging
250mg
Price
$38
Updated
2021/12/16
ChemScene
Product number
CS-W005648
Product name
2-Iodobenzo[d]thiazole
Purity
99.96%
Packaging
1g
Price
$46
Updated
2021/12/16
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2-IODOBENZOTHIAZOLE Chemical Properties,Usage,Production

Synthesis

95-16-9

1123-99-5

The general procedure for the synthesis of 2-iodobenzothiazole from benzothiazole was as follows: benzothiazole (1 mmol, 135.9 mg) and perfluorobutyl iodide (1.1 mmol, 380.5 mg) were placed in a 10 mL round bottom flask. 5 mL of N,N-dimethylformamide and sodium tert-butoxide (0.5 mmol, 48.1 mg) were added. The reaction mixture was stirred at room temperature for 20 min and the progress of the reaction was monitored by thin layer chromatography (TLC). After completion of the reaction, the mixture was poured into water and extracted with dichloromethane. The organic phase was collected and dried with anhydrous sodium sulfate, followed by removal of dichloromethane by rotary evaporator to give the crude product. The crude product was purified by silica gel column chromatography using petroleum ether and ethyl acetate (v/v=30:1) as eluents to give 2-iodobenzothiazole (white solid, 257.6 mg, 99% yield). In addition, the crude product can also be purified by recrystallization: the crude product was first washed with cold water, filtered, and dissolved in ethanol (2 mL). After heating until complete dissolution, it was left to stand and slowly cooled to induce precipitation of crystals.

References

[1] Organic and Biomolecular Chemistry, 2018, vol. 16, # 6, p. 886 - 890
[2] Patent: CN107501023, 2017, A. Location in patent: Paragraph 0033; 0034
[3] Angewandte Chemie - International Edition, 2006, vol. 45, # 18, p. 2958 - 2961
[4] Chemical Communications, 2008, # 42, p. 5375 - 5377
[5] Chemistry - A European Journal, 2009, vol. 15, # 39, p. 10280 - 10290

2-IODOBENZOTHIAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-IODOBENZOTHIAZOLE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
2-Iodobenzo[d]thiazole 1123-99-5
Price
US $1.60-6.60/kg
Min. Order
1kg
Purity
99%
Supply Ability
100kg
Release date
2025-06-19
Zhuozhou Wenxi import and Export Co., Ltd
Product
2-IODOBENZOTHIAZOLE 1123-99-5
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-11
Zhuozhou Wenxi import and Export Co., Ltd
Product
2-IODOBENZOTHIAZOLE 1123-99-5
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-07-09