(9-(4-BROMOPHENYL))-9H-CARBAZOLE
- Product Name
- (9-(4-BROMOPHENYL))-9H-CARBAZOLE
- CAS No.
- 57102-42-8
- Chemical Name
- (9-(4-BROMOPHENYL))-9H-CARBAZOLE
- Synonyms
- 3-NBPC;9-(4-Bromophenyl)carbazole;9-(4-BroMophenyl)carbazole90%;9-(4-Bromophenyl)carbazole >N-(4-BroMophenyl)-9H-carbazole;9H-Carbazole,9-(4-broMophenyl)-;9-(4-Bromophenyl)carbazole (9-(4-BROMOPHENYL))-9H-CARBAZOLE;9-(4-Bromophenyl)-9H-carbazole 98%;9-(4-broMophenyl)-9H-carbazole 4BPC
- CBNumber
- CB12459465
- Molecular Formula
- C18H12BrN
- Formula Weight
- 322.2
- MOL File
- 57102-42-8.mol
(9-(4-BROMOPHENYL))-9H-CARBAZOLE Property
- Melting point:
- 147-151℃
- Boiling point:
- 452.7±37.0 °C(Predicted)
- Density
- 1.39±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- Solid
- color
- White to Light yellow
- Water Solubility
- Slightly soluble in water.
- InChIKey
- XSDKKRKTDZMKCH-UHFFFAOYSA-N
- CAS DataBase Reference
- 57102-42-8
Safety
- HS Code
- 29339900
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- B3554
- Product name
- 9-(4-Bromophenyl)carbazole
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $41
- Updated
- 2025/07/31
- Product number
- B3554
- Product name
- 9-(4-Bromophenyl)carbazole
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $119
- Updated
- 2025/07/31
- Product number
- FB42951
- Product name
- (9-(4-Bromophenyl))-9H-carbazole
- Packaging
- 5G
- Price
- $60
- Updated
- 2021/12/16
- Product number
- JK1023050
- Product name
- 9-(4-Bromophenyl)carbazole
- Purity
- 98%
- Packaging
- 1g
- Price
- $84
- Updated
- 2021/12/16
- Product number
- FB42951
- Product name
- (9-(4-Bromophenyl))-9H-carbazole
- Packaging
- 10g
- Price
- $100
- Updated
- 2021/12/16
(9-(4-BROMOPHENYL))-9H-CARBAZOLE Chemical Properties,Usage,Production
Chemical Properties
White to light yellow solid
Uses
It plays an important role as intermediate for pharmaceutical, organic synthesis and organic light-emitting diode(OLED).
Synthesis
106-37-6
86-74-8
57102-42-8
Step 2: Synthesis of 4-(carbazol-9-yl)diphenylamine (abbreviation: YGA); In Step 2, YGA was synthesized according to (i) and (ii) shown below. (i) Synthesis of 9-(4-bromophenyl)carbazole; First, 56 g (240 mmol) of 1,4-dibromobenzene, 31 g (180 mmol) of carbazole, 4.6 g (24 mmol) of copper iodide, 16 g (480 mmol) of potassium carbonate and 2.1 g (8 mmol) of 18-crown-6-ether were added to a 300 mL three-necked flask and air displaced with nitrogen. 66 g (480 mmol) of potassium carbonate and 2.1 g (8 mmol) of 18-crown-6-ether were added to a 300 mL three-necked flask and the air in the flask was replaced with nitrogen. Subsequently, 8 mL of N,N-dimethylpropyleneurea (abbreviation: DMPU) was added to the flask and the reaction mixture was stirred at 180 °C for 6 hours. After completion of the reaction, the mixture was cooled to room temperature and the precipitate was removed by filtration. The filtrate was washed sequentially with dilute hydrochloric acid, saturated aqueous sodium bicarbonate solution and saturated aqueous sodium chloride solution, and then dried with anhydrous magnesium sulfate. After drying, the solution was naturally filtered and concentrated, and the resulting oil was purified by silica gel column chromatography (eluent: hexane/ethyl acetate = 9:1) and finally recrystallized with chloroform and hexane. Finally, 21 g of light brown plate-like crystals of the target product 9-(4-bromophenyl)carbazole were obtained in 35% yield.
References
[1] Chemistry Letters, 2008, vol. 37, # 9, p. 986 - 987
[2] Patent: CN106883163, 2017, A. Location in patent: Paragraph 0030; 0031; 0032; 0033
[3] New Journal of Chemistry, 2010, vol. 34, # 7, p. 1317 - 1322
[4] Patent: CN105585577, 2016, A. Location in patent: Paragraph 0220; 0221; 0222; 0223; 0224
[5] Patent: EP2292618, 2011, A1. Location in patent: Page/Page column 17
(9-(4-BROMOPHENYL))-9H-CARBAZOLE Preparation Products And Raw materials
Raw materials
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View Lastest Price from (9-(4-BROMOPHENYL))-9H-CARBAZOLE manufacturers
- Product
- (9-(4-BROMOPHENYL))-9H-CARBAZOLE 57102-42-8
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98.0%
- Supply Ability
- 10000KGS
- Release date
- 2025-05-16
- Product
- 9-(4-Bromophenyl)carbazole 57102-42-8
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-10-25
- Product
- (9-(4-BROMOPHENYL))-9H-CARBAZOLE 57102-42-8
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1000KGS
- Release date
- 2023-04-24