ChemicalBook > CAS DataBase List > PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-

PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-

Product Name
PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
CAS No.
60703-46-0
Chemical Name
PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
Synonyms
2,4,6-trichloro-5-MethoxypyriMidine;PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
CBNumber
CB12459915
Molecular Formula
C5H3Cl3N2O
Formula Weight
213.45
MOL File
60703-46-0.mol
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PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Property

Melting point:
67-68℃ (water, 50% ethanol )
Boiling point:
255.2±35.0 °C(Predicted)
Density 
1.572±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
-6.98±0.39(Predicted)
Appearance
White to yellow Solid
InChI
InChI=1S/C5H3Cl3N2O/c1-11-2-3(6)9-5(8)10-4(2)7/h1H3
InChIKey
BXDZWBOGMCNUSE-UHFFFAOYSA-N
SMILES
C1(Cl)=NC(Cl)=C(OC)C(Cl)=N1
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
T773755
Product name
2,4,6-Trichloro-5-methoxypyrimidine
Packaging
100mg
Price
$385
Updated
2021/12/16
Matrix Scientific
Product number
118777
Product name
2,4,6-Trichloro-5-methoxypyrimidine
Purity
>97%
Packaging
500mg
Price
$772
Updated
2021/12/16
Matrix Scientific
Product number
118777
Product name
2,4,6-Trichloro-5-methoxypyrimidine
Purity
>97%
Packaging
1g
Price
$1042
Updated
2021/12/16
AK Scientific
Product number
9071AB
Product name
2,4,6-Trichloro-5-methoxypyrimidine
Packaging
5g
Price
$2548
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0362621
Product name
2,4,6-TRICHLORO-5-METHOXYPYRIMIDINE
Purity
95.00%
Packaging
5MG
Price
$495.45
Updated
2021/12/16
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PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Chemical Properties,Usage,Production

Synthesis

71720-62-2

60703-46-0

Step 2: 2,4,6-Trichloro-5-methoxypyrimidine-6-hydroxy-5-methoxy-1H-pyrimidine-2,4-dione sodium salt (21 mmol) was suspended in phosphoryl chloride (20 mL). The mixture was dispensed in two 20 mL microwave reaction vials. The reaction mixture was heated at 130-140 °C (pressure about 10-12 bar) for 30 min (significant pressure rise was observed) using microwave radiation. After the reaction mixtures were cooled, they were carefully combined and slowly poured into water preheated to about 40°C. The resulting mixture was extracted twice with ethyl acetate, the organic phases were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 2,4,6-trichloro-5-methoxypyrimidine as a yellow/brown crystalline solid (3.75 g, 84% yield).1H NMR (CDCl3): δ 3.98 (s, 3H).

References

[1] Patent: WO2012/82997, 2012, A1. Location in patent: Page/Page column 84

PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Preparation Products And Raw materials

Raw materials

Preparation Products

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PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Suppliers

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View Lastest Price from PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- manufacturers

Career Henan Chemical Co
Product
PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- 60703-46-0
Price
US $3.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
200KG
Release date
2020-03-23

60703-46-0, PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-Related Search:


  • PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
  • 2,4,6-trichloro-5-MethoxypyriMidine
  • 60703-46-0