PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
- Product Name
- PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
- CAS No.
- 60703-46-0
- Chemical Name
- PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
- Synonyms
- 2,4,6-trichloro-5-MethoxypyriMidine;PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY-
- CBNumber
- CB12459915
- Molecular Formula
- C5H3Cl3N2O
- Formula Weight
- 213.45
- MOL File
- 60703-46-0.mol
PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Property
- Melting point:
- 67-68℃ (water, 50% ethanol )
- Boiling point:
- 255.2±35.0 °C(Predicted)
- Density
- 1.572±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -6.98±0.39(Predicted)
- Appearance
- White to yellow Solid
- InChI
- InChI=1S/C5H3Cl3N2O/c1-11-2-3(6)9-5(8)10-4(2)7/h1H3
- InChIKey
- BXDZWBOGMCNUSE-UHFFFAOYSA-N
- SMILES
- C1(Cl)=NC(Cl)=C(OC)C(Cl)=N1
N-Bromosuccinimide Price
- Product number
- T773755
- Product name
- 2,4,6-Trichloro-5-methoxypyrimidine
- Packaging
- 100mg
- Price
- $385
- Updated
- 2021/12/16
- Product number
- 118777
- Product name
- 2,4,6-Trichloro-5-methoxypyrimidine
- Purity
- >97%
- Packaging
- 500mg
- Price
- $772
- Updated
- 2021/12/16
- Product number
- 118777
- Product name
- 2,4,6-Trichloro-5-methoxypyrimidine
- Purity
- >97%
- Packaging
- 1g
- Price
- $1042
- Updated
- 2021/12/16
- Product number
- 9071AB
- Product name
- 2,4,6-Trichloro-5-methoxypyrimidine
- Packaging
- 5g
- Price
- $2548
- Updated
- 2021/12/16
- Product number
- HCH0362621
- Product name
- 2,4,6-TRICHLORO-5-METHOXYPYRIMIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.45
- Updated
- 2021/12/16
PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Chemical Properties,Usage,Production
Synthesis
71720-62-2
60703-46-0
Step 2: 2,4,6-Trichloro-5-methoxypyrimidine-6-hydroxy-5-methoxy-1H-pyrimidine-2,4-dione sodium salt (21 mmol) was suspended in phosphoryl chloride (20 mL). The mixture was dispensed in two 20 mL microwave reaction vials. The reaction mixture was heated at 130-140 °C (pressure about 10-12 bar) for 30 min (significant pressure rise was observed) using microwave radiation. After the reaction mixtures were cooled, they were carefully combined and slowly poured into water preheated to about 40°C. The resulting mixture was extracted twice with ethyl acetate, the organic phases were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 2,4,6-trichloro-5-methoxypyrimidine as a yellow/brown crystalline solid (3.75 g, 84% yield).1H NMR (CDCl3): δ 3.98 (s, 3H).
References
[1] Patent: WO2012/82997, 2012, A1. Location in patent: Page/Page column 84
PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Preparation Products And Raw materials
Raw materials
Preparation Products
PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- Suppliers
- Tel
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- info@chemsworth.com
- Country
- India
- ProdList
- 6700
- Advantage
- 30
- Tel
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- Fax
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- sales@ajchem.in
- Country
- India
- ProdList
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- Advantage
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View Lastest Price from PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- manufacturers
- Product
- PYRIMIDINE, 2,4,6-TRICHLORO-5-METHOXY- 60703-46-0
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200KG
- Release date
- 2020-03-23