BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER

Product Name: BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER
CAS No.: 199328-35-3
Chemical Name: BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER
Synonyms: Ethyl 2-(4-bromo-2-nitrophenyl);ethyl 4-bromo-2-nitrophenylacetate;2-(4-bromo-2-nitrophenyl)acetic acid ethyl ester;(4-Bromo-2-nitro-phenyl)-acetic acid ethyl ester;BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER
CBNumber: CB12467929
Molecular Formula: C10H10BrNO4
Formula Weight: 288.09
MOL File: 199328-35-3.mol

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BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER Property

Boiling point:: 345℃
Density: 1.542
Flash point:: 163℃
storage temp.: Sealed in dry,Room Temperature
Appearance: Brown to orange Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: Z4371
Product name: Ethyl2-(4-bromo-2-nitrophenyl)acetate
Packaging: 1g
Price: $172
Updated: 2021/12/16

Matrix Scientific

Product number: 126662
Product name: Ethyl2-(4-bromo-2-nitrophenyl)acetate
Purity: >95%
Packaging: 1g
Price: $450
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0368710
Product name: ETHYL-2-(4-BROMO-2-NITROPHENYL)ACETATE
Purity: 95.00%
Packaging: 5MG
Price: $496.56
Updated: 2021/12/16

Ambeed

Product number: A238474
Product name: Ethyl2-(4-bromo-2-nitrophenyl)acetate
Purity: 98%
Packaging: 250mg
Price: $30
Updated: 2021/12/16

Advanced Chemicals Intermediatesced Chemicals Intermediates

Product number: ACI-06401
Product name: (4-Bromo-2-nitro-phenyl)-aceticacidethylester
Purity: 95%+
Packaging: 250mg
Price: $37.7
Updated: 2021/12/16

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BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER Chemical Properties,Usage,Production

Synthesis

64-17-5

6127-11-3

199328-35-3

General procedure for the synthesis of ethyl 4-bromo-2-nitrophenylacetate from ethanol and 2-(4-bromo-2-nitrophenyl)acetic acid: to a solution of 2-(4-bromo-2-nitrophenyl)acetic acid (7.00 g, 27.0 mmol) in ethanol (60 mL) was slowly added concentrated sulfuric acid (1 mL). The reaction mixture was heated to reflux and maintained for 2 hours. Upon completion of the reaction, the reaction mixture was concentrated under reduced pressure. The concentrated residue was dissolved in ethyl acetate (250 mL) and separated by extraction with saturated sodium carbonate solution (50 mL). The organic layer was washed sequentially with saturated sodium carbonate solution (50 mL) and brine (50 mL). The organic layer was dried over anhydrous sodium sulfate and concentrated under reduced pressure to give ethyl 4-bromo-2-nitrophenylacetate (8.00 g, 98% yield) as an ester liquid.

References

[1] Patent: WO2005/63767, 2005, A2. Location in patent: Page/Page column 44
[2] Patent: US2007/78147, 2007, A1. Location in patent: Page/Page column 72
[3] Patent: WO2008/73480, 2008, A1. Location in patent: Page/Page column 27; 28
[4] ACS Medicinal Chemistry Letters, 2012, vol. 3, # 2, p. 140 - 145
[5] Patent: WO2006/52936, 2006, A2. Location in patent: Page/Page column 48

BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER Suppliers

China 48 India 3 United Kingdom 1 United States 6 Global 58

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199328-35-3, BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTERRelated Search:

Benzeneacetic acid, 4-bromo-3-chloro-, ethyl ester ethyl 2-(5-amino-2-chlorophenyl)acetate ethyl 3-chloro-4-nitrophenylacetate ethyl 4-amino-3-trifluoromethylphenylacetate Ethyl 2,3-difluoro-6-nitrophenylacetic acid ethyl 5-methoxy-2-(trifluoromethyl)phenylacetate ethyl 2-chloro-5-methylphenylacetic acid ethyl 4-nitro-3-trifluoromethylphenylacetate (2-CYANO-PHENYL)-ACETIC ACID ETHYL ESTER ethyl 4-cyano-3-(trifluoromethyl)phenyacetate ethyl 2-chloro-4-trifluoromethylphenylacetate (4-AMino-3-chloro-phenyl)-acetic acid ethyl ester ethyl 2-(3-chloro-4-fluorophenyl)acetate ethyl 4-bromo-2,5-difluorophenylacetic acid ethyl 2-(2-broMo-4-(trifluoroMethyl)phenyl)acetate

BENZENEACETIC ACID, 4-BROMO-2-NITRO-, ETHYL ESTER

(4-Bromo-2-nitro-phenyl)-acetic acid ethyl ester

Ethyl 2-(4-bromo-2-nitrophenyl)

2-(4-bromo-2-nitrophenyl)acetic acid ethyl ester

ethyl 4-bromo-2-nitrophenylacetate

199328-35-3