ChemicalBook > CAS DataBase List > 1-(4-(Bromomethyl)phenyl)ethanone
1-(4-(Bromomethyl)phenyl)ethanone
- Product Name
- 1-(4-(Bromomethyl)phenyl)ethanone
- CAS No.
- 51229-51-7
- Chemical Name
- 1-(4-(Bromomethyl)phenyl)ethanone
- Synonyms
- 1-(4-(Bromomethyl);4-Acetylbenzyl bromide;p-Acetylbenzyl bromide;4'-BROMOMETHYLACETOPHENONE;p-(Bromomethyl)acetophenone;4’-(Bromomethyl)acetophenone;1-(4-(Bromomethyl)phenyl)ethanone;1-[4-(broMoMethyl)phenyl]ethan-1-one;Ethanone, 1-[4-(broMoMethyl)phenyl]-
- CBNumber
- CB12470019
- Molecular Formula
- C9H9BrO
- Formula Weight
- 213.07
- MOL File
- 51229-51-7.mol
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1-(4-(Bromomethyl)phenyl)ethanone Property
- Melting point:
- 38.5-40.0℃
- Boiling point:
- 134-136℃ (5 Torr)
- Density
- 1.416±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- form
- Solid
- color
- Off-White
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Safety
- HS Code
- 2914390090
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
TRC
- Product number
- B697458
- Product name
- 1-(4-(Bromomethyl)phenyl)ethanone
- Packaging
- 5g
- Price
- $140
- Updated
- 2021/12/16
AK Scientific
- Product number
- W6622
- Product name
- 1-(4-(Bromomethyl)phenyl)ethanone
- Packaging
- 5g
- Price
- $141
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB31399
- Product name
- 1-(4-(Bromomethyl)phenyl)ethanone
- Packaging
- 2g
- Price
- $125
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB31399
- Product name
- 1-(4-(Bromomethyl)phenyl)ethanone
- Packaging
- 5G
- Price
- $200
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 076270
- Product name
- 1-(4-(Bromomethyl)phenyl)ethanone
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $14
- Updated
- 2021/12/16
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1-(4-(Bromomethyl)phenyl)ethanone Chemical Properties,Usage,Production
Uses
1-(4-(Bromomethyl)phenyl)ethanone is useful in the synthesis of series of dihydropyrimidine and thiopyrimidine derivatives as antiviral agents.
Synthesis
122-00-9
51229-51-7
General procedure for the synthesis of 1-(4-(bromomethyl)phenyl)ethanone from 4'-methylacetophenone: To a solution of 1-(4-methylphenyl)ethanone (600 mg, 4.47 mmol) in carbon tetrachloride (15 mL) was added sequentially N-bromosuccinimide (955 mg, 5.37 mmol) and benzoyl peroxide (31 mg, 0.13 mmol). The reaction mixture was heated to reflux for 3 hours, then cooled to room temperature and filtered. The filtrate was concentrated under reduced pressure to afford the target product 1-(4-(bromomethyl)phenyl)ethanone (683 mg, 71% yield) as a brown oil.LC-MS analysis showed the molecular ion peak [M+H]+ as 213.
References
[1] Journal of the American Chemical Society, 2006, vol. 128, # 5, p. 1404 - 1405
[2] Patent: CN103787966, 2016, B. Location in patent: Paragraph 0115-0117
[3] Journal of Medicinal Chemistry, 2017, vol. 60, # 18, p. 7703 - 7724
[4] Molecules, 2018, vol. 23, # 8, p. 1DUMMY
[5] Patent: CN107098791, 2017, A. Location in patent: Paragraph 0058-0060
1-(4-(Bromomethyl)phenyl)ethanone Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-(4-(Bromomethyl)phenyl)ethanone manufacturers
Career Henan Chemical Co
- Product
- 1-(4-(Bromomethyl)phenyl)ethanone 51229-51-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-20