1-(4-(Bromomethyl)phenyl)ethanone

Product Name: 1-(4-(Bromomethyl)phenyl)ethanone
CAS No.: 51229-51-7
Chemical Name: 1-(4-(Bromomethyl)phenyl)ethanone
Synonyms: 1-(4-(Bromomethyl);4-Acetylbenzyl bromide;p-Acetylbenzyl bromide;4'-BROMOMETHYLACETOPHENONE;p-(Bromomethyl)acetophenone;4’-(Bromomethyl)acetophenone;1-(4-(Bromomethyl)phenyl)ethanone;1-[4-(broMoMethyl)phenyl]ethan-1-one;Ethanone, 1-[4-(broMoMethyl)phenyl]-
CBNumber: CB12470019
Molecular Formula: C9H9BrO
Formula Weight: 213.07
MOL File: 51229-51-7.mol

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1-(4-(Bromomethyl)phenyl)ethanone Property

Melting point:: 38.5-40.0℃
Boiling point:: 134-136℃ (5 Torr)
Density: 1.416±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
solubility: Chloroform (Slightly), Methanol (Slightly)
form: Solid
color: Off-White

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Safety

HS Code: 2914390090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B697458
Product name: 1-(4-(Bromomethyl)phenyl)ethanone
Packaging: 5g
Price: $140
Updated: 2021/12/16

Matrix Scientific

Product number: 076270
Product name: 1-(4-(Bromomethyl)phenyl)ethanone
Purity: 95+%
Packaging: 250mg
Price: $14
Updated: 2021/12/16

Oakwood

Product number: 079582
Product name: 1-(4-(Bromomethyl)phenyl)ethanone
Purity: 97%
Packaging: 250mg
Price: $15
Updated: 2021/12/16

Matrix Scientific

Product number: 076270
Product name: 1-(4-(Bromomethyl)phenyl)ethanone
Purity: 95+%
Packaging: 500mg
Price: $22
Updated: 2021/12/16

Matrix Scientific

Product number: 076270
Product name: 1-(4-(Bromomethyl)phenyl)ethanone
Purity: 95+%
Packaging: 1g
Price: $34
Updated: 2021/12/16

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1-(4-(Bromomethyl)phenyl)ethanone Chemical Properties,Usage,Production

Uses

1-(4-(Bromomethyl)phenyl)ethanone is useful in the synthesis of series of dihydropyrimidine and thiopyrimidine derivatives as antiviral agents.

Synthesis

122-00-9

51229-51-7

General procedure for the synthesis of 1-(4-(bromomethyl)phenyl)ethanone from 4'-methylacetophenone: To a solution of 1-(4-methylphenyl)ethanone (600 mg, 4.47 mmol) in carbon tetrachloride (15 mL) was added sequentially N-bromosuccinimide (955 mg, 5.37 mmol) and benzoyl peroxide (31 mg, 0.13 mmol). The reaction mixture was heated to reflux for 3 hours, then cooled to room temperature and filtered. The filtrate was concentrated under reduced pressure to afford the target product 1-(4-(bromomethyl)phenyl)ethanone (683 mg, 71% yield) as a brown oil.LC-MS analysis showed the molecular ion peak [M+H]+ as 213.

References

[1] Journal of the American Chemical Society, 2006, vol. 128, # 5, p. 1404 - 1405
[2] Patent: CN103787966, 2016, B. Location in patent: Paragraph 0115-0117
[3] Journal of Medicinal Chemistry, 2017, vol. 60, # 18, p. 7703 - 7724
[4] Molecules, 2018, vol. 23, # 8, p. 1DUMMY
[5] Patent: CN107098791, 2017, A. Location in patent: Paragraph 0058-0060

1-(4-(Bromomethyl)phenyl)ethanone Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(4-(Bromomethyl)phenyl)ethanone Suppliers

China 94 India 1 United Kingdom 2 United States 6 Global 103

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View Lastest Price from 1-(4-(Bromomethyl)phenyl)ethanone manufacturers

Career Henan Chemical Co

Product: 1-(4-(Bromomethyl)phenyl)ethanone 51229-51-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-20

51229-51-7, 1-(4-(Bromomethyl)phenyl)ethanoneRelated Search:

1-(4-(Bromomethyl)phenyl)ethanone

4'-BROMOMETHYLACETOPHENONE

Ethanone, 1-[4-(broMoMethyl)phenyl]-

1-[4-(broMoMethyl)phenyl]ethan-1-one

1-(4-(Bromomethyl)

p-(Bromomethyl)acetophenone

p-Acetylbenzyl bromide

4-Acetylbenzyl bromide

4’-(Bromomethyl)acetophenone

51229-51-7