Methyl 4-(N-phenylcaramoyl)benzoate
- Product Name
- Methyl 4-(N-phenylcaramoyl)benzoate
- CAS No.
- 3814-10-6
- Chemical Name
- Methyl 4-(N-phenylcaramoyl)benzoate
- Synonyms
- BA-MMT;N-phenyl-p-carbomethoxybenzamide;Methyl 4-(phenylcarbaMoyl)benzoate;Methyl 4-(anilinocarbonyl)benzoate;METHYL 4-(N-PHENYLCARBAMOYL)BENZOATE;Methyl 4-(N-phenylcaramoyl)benzoate;Methyl 4-(Phenylcarbamoyl)benzoate >4-(Phenylcarbamoyl)benzoic Acid Methyl Ester;4-[(phenylamino)carbonyl]Benzoic acid methyl ester;Benzoic acid, 4-[(phenylamino)carbonyl]-, methyl ester
- CBNumber
- CB12473803
- Molecular Formula
- C15H13NO3
- Formula Weight
- 255.27
- MOL File
- 3814-10-6.mol
Methyl 4-(N-phenylcaramoyl)benzoate Property
- Melting point:
- 193℃
- Density
- 1.237
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Almost white
- CAS DataBase Reference
- 3814-10-6
Safety
- HS Code
- 2924.29.7790
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- M2637
- Product name
- Methyl 4-(Phenylcarbamoyl)benzoate
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $52
- Updated
- 2024/03/01
- Product number
- M2637
- Product name
- Methyl 4-(Phenylcarbamoyl)benzoate
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $148
- Updated
- 2025/07/31
- Product number
- M339073
- Product name
- Methyl4-(N-Phenylcaramoyl)benzoate
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- X0043
- Product name
- Methyl4-(N-phenylcaramoyl)benzoate
- Packaging
- 5g
- Price
- $142
- Updated
- 2021/12/16
- Product number
- A141662
- Product name
- Methyl 4-(Phenylcarbamoyl)benzoate
- Purity
- 98%
- Packaging
- 5g
- Price
- $17
- Updated
- 2021/12/16
Methyl 4-(N-phenylcaramoyl)benzoate Chemical Properties,Usage,Production
Chemical Properties
Grey white powder
Synthesis Reference(s)
The Journal of Organic Chemistry, 39, p. 3327, 1974 DOI: 10.1021/jo00937a004
Synthesis
7377-26-6
62-53-3
3814-10-6
To a 1 L three-necked round-bottomed flask equipped with a magnetic stirrer, a constant-pressure dropping funnel, an ice-water bath, a nitrogen protection system, a condenser tube, and a heating plate, 93.13 g of aniline, 42.30 g of sodium bicarbonate, 0.5 g of triethylamine, and 300 mL of tetrahydrofuran (THF) were added sequentially. The reaction mixture was cooled to below 10°C, followed by the slow dropwise addition of 100 g of methyl 4-chlorocarbonylbenzoate dissolved in 100 mL of THF. The reaction temperature was maintained at about 10°C during the dropwise addition.After the dropwise addition was completed, the reaction mixture was heated to reflux and the progress of the reaction was monitored by infrared spectroscopy (IR) (disappearance of the characteristic peak at 1780 cm-1 indicated completion of the reaction). After completion of the reaction, the reaction solution was diluted to 2 L with cold deionized water and stirring was continued for about 20 min. The solid product was collected by filtration and dried in an oven at 110°C. A final product of 105.6 g of the target product 4-methoxycarbonylbenzanilide was obtained in 82.2% yield.
References
[1] Patent: WO2015/42561, 2015, A1. Location in patent: Paragraph 0124
[2] Patent: WO2015/42563, 2015, A1. Location in patent: Paragraph 0124
[3] Patent: US9200142, 2015, B2. Location in patent: Page/Page column 36
Methyl 4-(N-phenylcaramoyl)benzoate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 4-(N-phenylcaramoyl)benzoate manufacturers
- Product
- Methyl 4-(N-phenylcaramoyl)benzoate 3814-10-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20t
- Release date
- 2024-07-16
- Product
- Methyl 4-(N-phenylcaraMoyl)benzoate 3814-10-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2019-12-31