Methyl 2-Fluoro-4-nitrophenylacetate

Product Name: Methyl 2-Fluoro-4-nitrophenylacetate
CAS No.: 337529-74-5
Chemical Name: Methyl 2-Fluoro-4-nitrophenylacetate
Synonyms: Methyl 2-Fluoro-4-nitrophenylacetate;2-fluoro-4-nitroBenzeneacetic acid methyl ester;Benzeneacetic acid, 2-fluoro-4-nitro-, Methyl ester
CBNumber: CB12500840
Molecular Formula: C9H8FNO4
Formula Weight: 213.16
MOL File: 337529-74-5.mol

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Methyl 2-Fluoro-4-nitrophenylacetate Property

Boiling point:: 309.0±27.0 °C(Predicted)
Density: 1.346±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M305563
Product name: Methyl2-(2-fluoro-4-nitrophenyl)acetate
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: M305563
Product name: Methyl2-(2-fluoro-4-nitrophenyl)acetate
Packaging: 1g
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: 6955AJ
Product name: Methyl2-fluoro-4-nitrophenylacetate
Packaging: 25g
Price: $904
Updated: 2021/12/16

Atlantic Research Chemicals

Product number: ES001498
Product name: Methyl2-(2-Fluoro-4-nitrophenyl)acetate
Purity: 95%
Packaging: 1gm:
Price: $130.78
Updated: 2021/12/16

Crysdot

Product number: CD12082029
Product name: Methyl2-(2-fluoro-4-nitrophenyl)acetate
Purity: 97%
Packaging: 5g
Price: $199
Updated: 2021/12/16

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Methyl 2-Fluoro-4-nitrophenylacetate Chemical Properties,Usage,Production

Synthesis

188975-47-5

337529-74-5

Step 2: Dimethyl 2-(2-fluoro-4-nitrophenyl)malonate (5.0 g, 18.5 mmol, 1.0 equiv) was dissolved in DMSO (30 mL) under stirring conditions. Subsequently, NaCl (1.07 g, 18.5 mmol, 1.0 eq.) and water (0.5 mL) were added to this solution and the reaction mixture was stirred at 120 °C for 3 hours. After completion of the reaction, the mixture was diluted with water (100 mL) and extracted with EtOAc (50 mL x 2). The combined organic layers were washed with brine, dried over anhydrous Na2SO4 and subsequently concentrated under reduced pressure to remove the solvent. The crude product was purified by column chromatography (eluent: petroleum ether/EtOAc, 19:1) to afford methyl 2-fluoro-4-nitrophenylacetate (2.5 g, 64%) as a viscous oil (TLC conditions: EtOAc/petroleum ether, 1:4, Rf value: 0.55).

References

[1] Patent: WO2013/68461, 2013, A1. Location in patent: Page/Page column 133
[2] Patent: WO2005/108397, 2005, A1. Location in patent: Page/Page column 37-38

Methyl 2-Fluoro-4-nitrophenylacetate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 2-Fluoro-4-nitrophenylacetate Suppliers

China 30 India 1 United States 6 Global 37

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View Lastest Price from Methyl 2-Fluoro-4-nitrophenylacetate manufacturers

Qingdao RENAS Polymer Material Co., Ltd.

Product: methyl 2-(2-fluoro-4-nitrophenyl)acetate 337529-74-5
Price: US $0.00/kg
Min. Order: 20kg
Purity: 99%
Supply Ability: 20 tons
Release date: 2025-05-12

337529-74-5, Methyl 2-Fluoro-4-nitrophenylacetateRelated Search:

Methyl 2-Fluoro-4-nitrophenylacetate

Benzeneacetic acid, 2-fluoro-4-nitro-, Methyl ester

2-fluoro-4-nitroBenzeneacetic acid methyl ester

337529-74-5