Methyl 2-Fluoro-4-nitrophenylacetate
- Product Name
- Methyl 2-Fluoro-4-nitrophenylacetate
- CAS No.
- 337529-74-5
- Chemical Name
- Methyl 2-Fluoro-4-nitrophenylacetate
- Synonyms
- Methyl 2-Fluoro-4-nitrophenylacetate;2-fluoro-4-nitroBenzeneacetic acid methyl ester;Benzeneacetic acid, 2-fluoro-4-nitro-, Methyl ester
- CBNumber
- CB12500840
- Molecular Formula
- C9H8FNO4
- Formula Weight
- 213.16
- MOL File
- 337529-74-5.mol
Methyl 2-Fluoro-4-nitrophenylacetate Property
- Boiling point:
- 309.0±27.0 °C(Predicted)
- Density
- 1.346±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M305563
- Product name
- Methyl2-(2-fluoro-4-nitrophenyl)acetate
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- M305563
- Product name
- Methyl2-(2-fluoro-4-nitrophenyl)acetate
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 6955AJ
- Product name
- Methyl2-fluoro-4-nitrophenylacetate
- Packaging
- 25g
- Price
- $904
- Updated
- 2021/12/16
- Product number
- ES001498
- Product name
- Methyl2-(2-Fluoro-4-nitrophenyl)acetate
- Purity
- 95%
- Packaging
- 1gm:
- Price
- $130.78
- Updated
- 2021/12/16
- Product number
- CD12082029
- Product name
- Methyl2-(2-fluoro-4-nitrophenyl)acetate
- Purity
- 97%
- Packaging
- 5g
- Price
- $199
- Updated
- 2021/12/16
Methyl 2-Fluoro-4-nitrophenylacetate Chemical Properties,Usage,Production
Synthesis
188975-47-5
337529-74-5
Step 2: Dimethyl 2-(2-fluoro-4-nitrophenyl)malonate (5.0 g, 18.5 mmol, 1.0 equiv) was dissolved in DMSO (30 mL) under stirring conditions. Subsequently, NaCl (1.07 g, 18.5 mmol, 1.0 eq.) and water (0.5 mL) were added to this solution and the reaction mixture was stirred at 120 °C for 3 hours. After completion of the reaction, the mixture was diluted with water (100 mL) and extracted with EtOAc (50 mL x 2). The combined organic layers were washed with brine, dried over anhydrous Na2SO4 and subsequently concentrated under reduced pressure to remove the solvent. The crude product was purified by column chromatography (eluent: petroleum ether/EtOAc, 19:1) to afford methyl 2-fluoro-4-nitrophenylacetate (2.5 g, 64%) as a viscous oil (TLC conditions: EtOAc/petroleum ether, 1:4, Rf value: 0.55).
References
[1] Patent: WO2013/68461, 2013, A1. Location in patent: Page/Page column 133
[2] Patent: WO2005/108397, 2005, A1. Location in patent: Page/Page column 37-38
Methyl 2-Fluoro-4-nitrophenylacetate Preparation Products And Raw materials
Raw materials
Preparation Products
Methyl 2-Fluoro-4-nitrophenylacetate Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from Methyl 2-Fluoro-4-nitrophenylacetate manufacturers
- Product
- methyl 2-(2-fluoro-4-nitrophenyl)acetate 337529-74-5
- Price
- US $0.00/kg
- Min. Order
- 20kg
- Purity
- 99%
- Supply Ability
- 20 tons
- Release date
- 2025-05-12