5-Nitro-3-(trifluoromethyl)-2-pyridinamine

Product Name: 5-Nitro-3-(trifluoromethyl)-2-pyridinamine
CAS No.: 1121056-94-7
Chemical Name: 5-Nitro-3-(trifluoromethyl)-2-pyridinamine
Synonyms: 5-Nitro-3-(trifluoroMethyl)pyridin-2-aMine;5-Nitro-3-(trifluoromethyl)-2-pyridinamine;5-Nitro-3-trifluoroMethyl-pyridin-2-ylaMine;2-Pyridinamine, 5-nitro-3-(trifluoromethyl)-
CBNumber: CB12534645
Molecular Formula: C6H4F3N3O2
Formula Weight: 207.11
MOL File: 1121056-94-7.mol

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5-Nitro-3-(trifluoromethyl)-2-pyridinamine Property

Boiling point:: 308℃
Density: 1.589
Flash point:: 140℃
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 0.09±0.49(Predicted)
Appearance: Off-white to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: N900995
Product name: 5-Nitro-3-(trifluoromethyl)pyridin-2-amine
Packaging: 50mg
Price: $110
Updated: 2021/12/16

Matrix Scientific

Product number: 093295
Product name: 5-Nitro-3-(trifluoromethyl)pyridin-2-amine
Purity: 95+%
Packaging: 250mg
Price: $473
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367523
Product name: 5-NITRO-3-(TRIFLUOROMETHYL)PYRIDIN-2-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $500.52
Updated: 2021/12/16

Matrix Scientific

Product number: 093295
Product name: 5-Nitro-3-(trifluoromethyl)pyridin-2-amine
Purity: 95+%
Packaging: 1g
Price: $975
Updated: 2021/12/16

Ambeed

Product number: A167408
Product name: 5-Nitro-3-(trifluoromethyl)pyridin-2-amine
Purity: 96%
Packaging: 100mg
Price: $45
Updated: 2021/12/16

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5-Nitro-3-(trifluoromethyl)-2-pyridinamine Chemical Properties,Usage,Production

Synthesis

183610-70-0

1121056-94-7

General procedure for the synthesis of 5-nitro-3-(trifluoromethyl)pyridin-2-amine from 2-amino-3-(trifluoromethyl)pyridine: 2-amino-3-(trifluoromethyl)pyridine (2 g, 12.34 mmol) was dissolved in concentrated sulfuric acid (10 mL) at 0 °C, and fuming nitric acid (0.56 mL, 12.34 mmol) was slowly added dropwise. After the dropwise addition, the reaction mixture was kept stirred at 0°C for 15 minutes, then brought to room temperature and continued to stir for 1 hour. After that, the reaction system was heated to 50 °C and maintained for 2 hours. Upon completion of the reaction, the mixture was cooled to room temperature and quenched by slowly pouring into ice water (200 mL). The precipitated solid product was collected by filtration and dried under high vacuum to afford 5-nitro-3-(trifluoromethyl)pyridin-2-amine (1.92 g, 75% yield). The structure of the product was confirmed by 1H NMR (d6-DMSO, 300 MHz) δ 8.02 (brs, 2H), 8.38 (d, 1H, J = 2.6 Hz), 9.04 (d, 1H, J = 2.6 Hz) and mass spectrum (ESI) m/z = 208 (MH+).

References

[1] Patent: WO2009/23179, 2009, A2. Location in patent: Page/Page column 240-241

5-Nitro-3-(trifluoromethyl)-2-pyridinamine Preparation Products And Raw materials

Raw materials

Preparation Products

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