2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate

Product Name: 2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate
CAS No.: 164162-36-1
Chemical Name: 2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate
Synonyms: Everolimus Impurity 12;Everolimus intermediate A2(Z);2-(tert-Butydilethylsily) oxyethyl;2-(t-ButyldiMethylsilyl)oxyethyl triflate;2-(tert-Butyldimethylsilyloxy)ethyl triflate;2-(t-Butyldimethylsilyloxy)EthylTrifluoromethanesulfonate;2-(tert-butyldiMethylsilyloxy)ethyl trifluoroMethanesulfonate;2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate;2-{[Dimethyl(2-methyl-2-propanyl)silyl]oxy}ethyl trifluoromethanesulfonate;Trifluoromethanesulfonic acid 2-[[(tert-butyl)dimethylsilyl]oxy]ethyl ester
CBNumber: CB12542770
Molecular Formula: C9H19F3O4SSi
Formula Weight: 308.39
MOL File: 164162-36-1.mol

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2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate Property

Boiling point:: 253℃
Density: 1.172
Flash point:: 107℃

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: ORS0003977
Product name: 2-((TERT-BUTYLDIMETHYLSILYL)OXY)ETHYL TRIFLUOROMETHANESULFONATE
Purity: 95.00%
Packaging: 5MG
Price: $499.02
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: ORS0003977
Product name: 2-((TERT-BUTYLDIMETHYLSILYL)OXY)ETHYL TRIFLUOROMETHANESULFONATE
Purity: 95.00%
Packaging: 250MG
Price: $1145.55
Updated: 2021/12/16

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2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate Chemical Properties,Usage,Production

Uses

2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate is used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis

The reaction was carried out under a nitrogen atmosphere. TBS- ethylene glycol prepared as per step 1 (85.10g, 0.48 mol) and 2, 6-Lutidine (84.28ml, 0.72 mol) were stirred in n-heptane (425ml) to give a clear solution which was then cooled to -15 to - 25°C. Trifluoromethanesulfonic anhydride (Tf2O) (99.74 ml, 0.590 mol) was added drop-wise over a period of 45 minutes to the n-heptane solution (white precipitate starts to form immediately) while maintaining the reaction at -15 to -25°C. The reaction mixture was kept at temperature between -15 to -25°C for 2 hours. The precipitate generated was filtered off. The filtrate was then evaporated up to ~2 volumes with respect to TBS-ethyiene glycol (~200 ml).

2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate Suppliers

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164162-36-1, 2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin MethanesulfonateRelated Search:

BIS(T-BUTYLDIMETHYLSILOXY)ETHANE Methanesulfonic acid, trifluoro-, 2-hydroxyethyl ester Ethyleneglycol bistriflate Everolimus Ring-Opening Impurity Everolimus Impurity 1 Everolimus Related Compound 3 Rapamycin EveroliMus-d4 Everolimus 2,6-di-tert-butyl-4-methylene-2,5-cyclohexadienone EveroliMus iMpurity Everolimus O-Ethyl Impurity Everolimus Related Compound 2

2-{[Dimethyl(2-methyl-2-propanyl)silyl]oxy}ethyl trifluoromethanesulfonate

Trifluoromethanesulfonic acid 2-[[(tert-butyl)dimethylsilyl]oxy]ethyl ester

2-(t-ButyldiMethylsilyl)oxyethyl triflate

Methanesulfonicacid,1,1,1-trifluoro-,2-[[(1,1-diMethylethyl)diMethylsilyl]oxy]ethylester

2-(t-Butyldimethylsilyloxy)EthylTrifluoromethanesulfonate

2-(tert-butyldiMethylsilyl )oxyl alcohol trifluorin Methanesulfonate

2-(tert-butyldiMethylsilyloxy)ethyl trifluoroMethanesulfonate

1,1,1-Trifluoromethanesulfonic acid 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl ester

Everolimus Impurity 12

2-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]ethyl 1,1,1-trifluoromethanesulfonate

Everolimus intermediate A2(Z)

2-(tert-Butydilethylsily) oxyethyl

2-(tert-Butyldimethylsilyloxy)ethyl triflate

164162-36-1

C9H19F3O4SSi