3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
- Product Name
- 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
- CAS No.
- 396731-40-1
- Chemical Name
- 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
- Synonyms
- N-Boc-3,5-dioxopiperidine;5-dioxopiperidine-1-carboxylate;tert-Butyl 3,5-dioxopiperidine-1-carboxylat;tert-butyl 3,5-dioxo-1-piperidinecarboxylate;3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester;1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-dimethylethyl e...;1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-diMethylethyl ester;3,5-dioxo-1-Piperidinecarboxylic acid 1,1-dimethylethyl ester (9CI ACI);1-Piperidinecarboxylic acid, 3,5-dioxo-, 1,1-dimethylethyl ester (9CI, ACI)
- CBNumber
- CB12618116
- Molecular Formula
- C10H15NO4
- Formula Weight
- 213.23
- MOL File
- 396731-40-1.mol
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester Property
- Boiling point:
- 346.2±32.0 °C(Predicted)
- Density
- 1.199±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- solid
- pka
- 9.72±0.20(Predicted)
- color
- Light yellow to yellow
- CAS DataBase Reference
- 396731-40-1
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B694530
- Product name
- tert-Butyl3,5-dioxopiperidine-1-carboxylate
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- FD71552
- Product name
- 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FD71552
- Product name
- 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- 5216AB
- Product name
- tert-Butyl3,5-dioxopiperidine-1-carboxylate
- Packaging
- 5g
- Price
- $134
- Updated
- 2021/12/16
- Product number
- FD71552
- Product name
- 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester
- Packaging
- 2g
- Price
- $150
- Updated
- 2021/12/16
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester Chemical Properties,Usage,Production
Uses
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
Synthesis
To a cooled (5 ??C) and stirred mixture of potassium 2-methyl-2-propoxide (29.7 g,0.27 mol) was added a solution of ethyl [A/-((1,1-dimethylethoxy)carbonyl),A/-(2-oxopropyl)]glycinate (65 g, 0.25 mol) in ethyl ether (200 ml) over a period of 1.5 h. The re- sulting mixture was stirred for an additional 3 h, and the formed precipitate was filtered offand washed with ethyl ether (2 x 100 ml). The solid was dissolved in water (150 ml), andacetic acid was added to adjust the pH to 4. The product was filtered, washed with water (2x 50 ml) and air dried to furnish 1 -[(1,1 -dimethylethoxy)carbonyl]-3,5-dioxopiperidine (28 g,52 %).>xxN'TOHPLC-MS: m/z: 158 (M+H-56).1H-NMR (DMSO-d6): 81.48 (9H, s), 4.03 (4H, s), 5.38 (1 H, s).
3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester manufacturers
- Product
- 3,5-Dioxo-piperidine-1-carboxylicacidtert-butylester 396731-40-1
- Price
- US $1.00/KG
- Min. Order
- 1G
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2018-08-15