9-(4-broMophenyl)-10-phenylanthracene
Uses- Product Name
- 9-(4-broMophenyl)-10-phenylanthracene
- CAS No.
- 625854-02-6
- Chemical Name
- 9-(4-broMophenyl)-10-phenylanthracene
- Synonyms
- 9-phenyl-10-(4-bromophenyl)anthracene;9-(4-broMophenyl)-10-phenylanthracene;Anthracene, 9-(4-bromophenyl)-10-phenyl-;9-(4-Bromophenyl)-10-phenylanthracene >2-(Dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1'-;9-(4-broMophenyl)-10-phenylanthracene ISO 9001:2015 REACH
- CBNumber
- CB12645275
- Molecular Formula
- C26H17Br
- Formula Weight
- 409.32
- MOL File
- 625854-02-6.mol
9-(4-broMophenyl)-10-phenylanthracene Property
- Melting point:
- 225.0 to 229.0 °C
- Boiling point:
- 505.4±19.0 °C(Predicted)
- Density
- 1.344±0.06 g/cm3 (20 ºC 760 Torr)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- slightly sol. in Toluene
- form
- powder to crystal
- color
- White to Light yellow to Green
- CAS DataBase Reference
- 625854-02-6
Safety
- HS Code
- 2903998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
H412Harmful to aquatic life with long lasting effects
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P273Avoid release to the environment.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B4475
- Product name
- 9-(4-Bromophenyl)-10-phenylanthracene
- Purity
- >98.0%(GC)
- Packaging
- 200mg
- Price
- $55
- Updated
- 2025/07/31
- Product number
- B4475
- Product name
- 9-(4-Bromophenyl)-10-phenylanthracene
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $190
- Updated
- 2025/07/31
- Product number
- B807835
- Product name
- 9-(4-Bromophenyl)-10-phenylanthracene
- Packaging
- 100mg
- Price
- $90
- Updated
- 2021/12/16
- Product number
- B807835
- Product name
- 9-(4-Bromophenyl)-10-phenylanthracene
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 1600-9-31
- Product name
- 9-(4-Bromophenyl)-10-phenylanthracene
- Purity
- 98%
- Packaging
- 1g
- Price
- $90
- Updated
- 2021/12/16
9-(4-broMophenyl)-10-phenylanthracene Chemical Properties,Usage,Production
Uses
9-(4-Bromophenyl)-10-phenylanthracene (cas# 625854-02-6) is a useful research chemical.
Synthesis
5467-74-3
150712-74-6
625854-02-6
The general procedure for the synthesis of 9-(4-bromophenyl)-10-phenylanthracene from 4-bromophenylboronic acid and compound (CAS:150712-74-6) is as follows: (iv) Synthesis of 9-(4-bromophenyl)-10-phenylanthracene In a 100 mL three-necked flask, 5.3 g (14 mmol) of 9-iodo-10-phenylanthracene, 2.9 g (14 mmol) of 4-bromophenylboronic acid and 0.18 g (0.15 mmol) of tetrakis(triphenylphosphine)palladium(0) were added sequentially. Subsequently, the atmosphere in the flask was replaced with nitrogen. To the reaction system was added 30 mL of toluene and 15 mL (31 mmol) of 2.0 mol/L aqueous sodium carbonate solution. The mixture was reacted at reflux for 10 h at 110 °C. Upon completion of the reaction, the precipitate in the reaction mixture was collected by diafiltration. The resulting solid was dissolved in toluene and filtered sequentially by filtration through Florisil, diatomaceous earth and alumina. The filtrate was concentrated and the resulting solid was recrystallized using a solvent mixture of chloroform and hexane. The final 4.1 g of the target product, 9-(4-bromophenyl)-10-phenylanthracene, was obtained as a light yellow powdery solid in 72% yield. The following is the synthetic scheme of 9-(4-bromophenyl)-10-phenylanthracene (synthetic scheme b-4).
References
[1] Patent: US2008/81934, 2008, A1. Location in patent: Page/Page column 36
[2] Patent: WO2006/104221, 2006, A1. Location in patent: Page/Page column 61-62
[3] Patent: WO2007/13537, 2007, A1. Location in patent: Page/Page column 95-96
[4] Patent: WO2007/7885, 2007, A1. Location in patent: Page/Page column 54
[5] Patent: US2007/96639, 2007, A1. Location in patent: Page/Page column 111
9-(4-broMophenyl)-10-phenylanthracene Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9-(4-broMophenyl)-10-phenylanthracene manufacturers
- Product
- 9-(4-broMophenyl)-10-phenylanthracene 625854-02-6
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-16
- Product
- 9-(4-Bromophenyl)-10-phenylanthracene 625854-02-6
- Price
- US $188.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-01-05
- Product
- 9-(4-broMophenyl)-10-phenylanthracene 625854-02-6
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-09-21