9-Bromo-10-(2-naphthyl)anthracene
- Product Name
- 9-Bromo-10-(2-naphthyl)anthracene
- CAS No.
- 474688-73-8
- Chemical Name
- 9-Bromo-10-(2-naphthyl)anthracene
- Synonyms
- 9-BroMo-10-naphthalen-2-yl-anthracene;BA2N;9-Bromo-10-(2-naphth;9-BroMo-10-naphthalen-2-yl-ant;9-Bromo-10-(2-naphthyl)anthracene;9-bromo-10-(2-naphtyl)-anthracene;10-(2-Naphthyl)-9-bromoanthracene;9-BroMo-10-(naphth-2-yl)anthracene;9-Bromo-10-(2-phthalenyl)anthracene;9-Bromo-10-(naphthyl-2-yl)anthracene
- CBNumber
- CB1948071
- Molecular Formula
- C24H15Br
- Formula Weight
- 383.28
- MOL File
- 474688-73-8.mol
9-Bromo-10-(2-naphthyl)anthracene Property
- Melting point:
- 169.0 to 173.0 °C
- Boiling point:
- 518.9±19.0 °C(Predicted)
- Density
- 1.402±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- soluble in Toluene
- form
- powder to crystal
- color
- White to Yellow to Green
- InChI
- InChI=1S/C24H15Br/c25-24-21-11-5-3-9-19(21)23(20-10-4-6-12-22(20)24)18-14-13-16-7-1-2-8-17(16)15-18/h1-15H
- InChIKey
- FKIFDWYMWOJKTQ-UHFFFAOYSA-N
- SMILES
- C1=C2C(C(C3=CC=C4C(=C3)C=CC=C4)=C3C(=C2Br)C=CC=C3)=CC=C1
- CAS DataBase Reference
- 474688-73-8
Safety
- HS Code
- 2903.99.8001
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B4426
- Product name
- 9-Bromo-10-(2-naphthyl)anthracene
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $56
- Updated
- 2025/07/31
- Product number
- B4426
- Product name
- 9-Bromo-10-(2-naphthyl)anthracene
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $189
- Updated
- 2025/07/31
- Product number
- B698300
- Product name
- 9-Bromo-10-(2-naphthyl)anthracene
- Packaging
- 250mg
- Price
- $40
- Updated
- 2021/12/16
- Product number
- R503
- Product name
- 9-Bromo-10-(2-naphthyl)anthracene
- Packaging
- 5g
- Price
- $206
- Updated
- 2021/12/16
- Product number
- HCH0037094
- Product name
- 9-BROMO-10-(2-NAPHTHYL)ANTHRACENE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $909.56
- Updated
- 2021/12/16
9-Bromo-10-(2-naphthyl)anthracene Chemical Properties,Usage,Production
Chemical Properties
off-white powder
Uses
9-Bromo-10-(2-naphthyl)anthracene is a reagent used in the determination of amines.
Synthesis
7424-72-8
474688-73-8
The general procedure for the synthesis of 9-bromo-10-(2-naphthalenyl)anthracene from 9-(naphthalen-2-yl)anthracene was as follows: 9-(2-naphthalenyl)anthracene (2.7 g, 8.9 mmol) was suspended in anhydrous N,N-dimethylformamide (DMF, 50 mL). To this suspension was slowly added anhydrous DMF solution (6 mL) dissolved in N-bromosuccinimide (NBS, 1.7 g, 9.6 mmol, 1.1 equiv). The resulting mixture was stirred and reacted for 10 h at room temperature and then left to stand overnight. Upon completion of the reaction, the reaction mixture was diluted with deionized water (50 mL). The resulting yellowish solid product was separated by filtration and washed with methanol to give the final target compound 9-bromo-10-(2-naphthyl)anthracene (3.2 g, 94% yield). The structure of the product was confirmed by 1H-NMR (CDCl3, TMS) with chemical shifts δ: 7.2-7.7 (9H, m), 7.8-8.1 (4H, m), 8.62 (2H, d, J = 8 Hz).
References
[1] Patent: WO2007/102683, 2007, A1. Location in patent: Page/Page column 52
[2] Patent: EP1496041, 2005, A1. Location in patent: Page 22
[3] Chemical Communications, 2013, vol. 49, # 41, p. 4664 - 4666
[4] Patent: KR101548370, 2015, B1. Location in patent: Paragraph 0117; 0118; 0121; 0122
[5] Patent: US2005/245752, 2005, A1. Location in patent: Page/Page column 8
9-Bromo-10-(2-naphthyl)anthracene Preparation Products And Raw materials
Raw materials
Preparation Products
9-Bromo-10-(2-naphthyl)anthracene Suppliers
- Tel
- 027-027-87915283 15972929998
- Fax
- 027-87915283
- sales@sunshine-oled.com
- Country
- China
- ProdList
- 684
- Advantage
- 58
- Tel
- 0371-67759225 13526468238
- sales@hqmat.com
- Country
- China
- ProdList
- 589
- Advantage
- 58
- Tel
- 0550-5261666 19901505185
- Fax
- 0550-5261919
- sales@sholonchem.com
- Country
- China
- ProdList
- 213
- Advantage
- 58
- Tel
- 0371-61280670 15638139892
- Fax
- 0371-61280670
- dongguinan@chuanganchem.com
- Country
- China
- ProdList
- 574
- Advantage
- 58
- Tel
- 400-6106006
- Fax
- 021-67582001/03/05
- saleschina@alfa-asia.com
- Country
- China
- ProdList
- 30123
- Advantage
- 84
- Tel
- 021-67121386
- Fax
- 021-67121385
- Sales-CN@TCIchemicals.com
- Country
- China
- ProdList
- 24529
- Advantage
- 81
- Tel
- 18515581800 18501085097
- Fax
- 010-89508210
- sales.bj@hwrkchemical.com
- Country
- China
- ProdList
- 9400
- Advantage
- 55
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 0431-85877181
- Fax
- 0431-85804772
- sales@jl-oled.com
- Country
- China
- ProdList
- 154
- Advantage
- 68
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9310
- Advantage
- 66
View Lastest Price from 9-Bromo-10-(2-naphthyl)anthracene manufacturers
- Product
- 9-Bromo-10-(2-naphthyl)anthracene 474688-73-8
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-09-27
- Product
- 9-Bromo-10-(2-naphthyl)anthracene 474688-73-8
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG /month
- Release date
- 2021-11-19
- Product
- 9-Bromo-10-(2-naphthyl)anthracene 474688-73-8
- Price
- US $188.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-01-05