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9-phenylanthracene

Product Name
9-phenylanthracene
CAS No.
602-55-1
Chemical Name
9-phenylanthracene
Synonyms
NSC 90796;9-phenylantracene;9-PHENYLANTHRACENE;Phenylanthracene,98%;anthracene,9-phenyl-;9-Phenylanthracene97%;9-Phenylanthracene>9-Phenylanthracene,98%;9-Phenylanthracene 97%;9-PHENYLANTHRACENE OEKANAL
CBNumber
CB8778824
Molecular Formula
C20H14
Formula Weight
254.33
MOL File
602-55-1.mol
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9-phenylanthracene Property

Melting point:
153-155 °C (lit.)
Boiling point:
417 °C (lit.)
Density 
1.1180 (estimate)
refractive index 
1.7040 (estimate)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Slightly), Ethyl Acetate (Slightly)
form 
Solid
color 
Off-white to pale brown
Sensitive 
Light Sensitive
BRN 
1910570
CAS DataBase Reference
602-55-1(CAS DataBase Reference)
EPA Substance Registry System
Anthracene, 9-phenyl- (602-55-1)
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Safety

Hazard Codes 
N
Risk Statements 
50/53
Safety Statements 
60-61
RIDADR 
UN 3077 9/PG 3
WGK Germany 
3
HazardClass 
9
HS Code 
29029090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
P18004
Product name
9-Phenylanthracene
Purity
98%
Packaging
5g
Price
$183.6
Updated
2024/03/01
Sigma-Aldrich
Product number
P18004
Product name
9-Phenylanthracene
Purity
98%
Packaging
1g
Price
$86.3
Updated
2023/06/20
TCI Chemical
Product number
P0138
Product name
9-Phenylanthracene
Purity
>98.0%(GC)
Packaging
1g
Price
$113
Updated
2024/03/01
TCI Chemical
Product number
P0138
Product name
9-Phenylanthracene
Purity
>98.0%(GC)
Packaging
5g
Price
$394
Updated
2024/03/01
Alfa Aesar
Product number
H64419
Product name
9-Phenylanthracene, 98%
Packaging
1g
Price
$23.8
Updated
2021/12/16
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9-phenylanthracene Chemical Properties,Usage,Production

Chemical Properties

Pale Yellow Plates

Uses

9-Phenylanthracene is used to synthesize organic light-emitting material intermediates.

Preparation

The synthesis of 9-phenylanthracene involved mixing phenylboronic acid (2.13 g, 17.49 mmol), 9-bromoanthracene (3 g, 11.66 mmol), Pd(PPh3)4 (140 mg, 0.12 mmol), K2CO3 (16 mL, 2 M), and ethanol (8 mL) in a 100 mL flask with anhydrous toluene (32 mL). The mixture was refluxed for 48 h under nitrogen. After cooled to room temperature, the reaction mixture was quenched with dilute hydrochloric acid solution and extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation. The crude product was further purified by silica gel column chromatography (CH2Cl2/petroleum ether (1:4,v/v)) to get a white powder (2.43 g, 81.9 %). 1H NMR (500 MHz, CDCl3) δ 8.53 (s, 1H), 8.08 (d, J = 8.5 Hz, 2H), 7.70 – 7.67 (m, 2H), 7.63 – 7.54 (m, 3H), 7.50 – 7.45 (m, 4H), 7.37 (ddd, J = 8.7, 6.5, 1.2 Hz, 2H). EI-MS (m/z): Calculated for C20H14: 254.33. Found [M+]: 253.02.

Synthesis of 9-phenylanthracene

Synthesis Reference(s)

Journal of the American Chemical Society, 79, p. 393, 1957 DOI: 10.1021/ja01559a042

Purification Methods

Chromatograph it on alumina in *C6H6 and recrystallise it from AcOH or toluene. [Beilstein 5 H 725, 5 II 639, 5 III 2462.]

9-phenylanthracene Preparation Products And Raw materials

Raw materials

Preparation Products

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9-phenylanthracene Suppliers

Suzhou A-Photoelectic Materials Co.,Ltd
Tel
18913195221
Fax
QQ2028380290
Email
szaw2018@163.com
Country
China
ProdList
293
Advantage
58
Henan Chuangan Optoelectronics Technology Co., Ltd.
Tel
0371-61280670 15638139892
Fax
0371-61280670
Email
2463687127@qq.com
Country
China
ProdList
493
Advantage
58
J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
3B Pharmachem (Wuhan) International Co.,Ltd.
Tel
821-50328103-801 18930552037
Fax
86-21-50328109
Email
3bsc@sina.com
Country
China
ProdList
15839
Advantage
69
Alfa Aesar
Tel
400-6106006
Fax
021-67582001/03/05
Email
saleschina@alfa-asia.com
Country
China
ProdList
30123
Advantage
84
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44689
Advantage
61
Jilin OLED Material Tech Co., Ltd
Tel
0431-85877181
Fax
0431-85804772
Email
sales@jl-oled.com
Country
China
ProdList
154
Advantage
68
Chemsky(shanghai)International Co.,Ltd.
Tel
021-50135380
Email
shchemsky@sina.com
Country
China
ProdList
32321
Advantage
50
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View Lastest Price from 9-phenylanthracene manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD
Product
9-phenylanthracene 602-55-1
Price
US $0.00/KG
Min. Order
1KG
Purity
98%min
Supply Ability
30tons/month
Release date
2023-04-07
Shanghai Daken Advanced Materials Co.,Ltd
Product
9-PHENYLANTHRACENE 602-55-1
Price
US $0.00/KG
Min. Order
1KG
Purity
98.00%
Supply Ability
150KG /month
Release date
2021-11-16
Hebei Xinsheng New Material Technology Co., LTD.
Product
9-phenylanthracene 602-55-1
Price
US $35.00-25.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 Ton
Release date
2023-09-22

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