9-phenylanthracene

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9-phenylanthracene

Product Name: 9-phenylanthracene
CAS No.: 602-55-1
Chemical Name: 9-phenylanthracene
Synonyms: NSC 90796;9-phenylantracene;9-PHENYLANTHRACENE;Phenylanthracene,98%;anthracene,9-phenyl-;9-Phenylanthracene97%;9-Phenylanthracene>9-Phenylanthracene,98%;9-Phenylanthracene 97%;9-PHENYLANTHRACENE OEKANAL
CBNumber: CB8778824
Molecular Formula: C20H14
Formula Weight: 254.33
MOL File: 602-55-1.mol

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9-phenylanthracene Property

Melting point:: 153-155 °C (lit.)
Boiling point:: 417 °C (lit.)
Density: 1.1180 (estimate)
refractive index: 1.7040 (estimate)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform (Slightly), Ethyl Acetate (Slightly)
form: Solid
color: Off-white to pale brown
Sensitive: Light Sensitive
BRN: 1910570
CAS DataBase Reference: 602-55-1(CAS DataBase Reference)
EPA Substance Registry System: Anthracene, 9-phenyl- (602-55-1)

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Safety

Hazard Codes: N
Risk Statements: 50/53
Safety Statements: 60-61
RIDADR: UN 3077 9/PG 3
WGK Germany: 3
HazardClass: 9
HS Code: 29029090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: P18004
Product name: 9-Phenylanthracene
Purity: 98%
Packaging: 5g
Price: $183.6
Updated: 2024/03/01

Sigma-Aldrich

Product number: P18004
Product name: 9-Phenylanthracene
Purity: 98%
Packaging: 1g
Price: $86.3
Updated: 2023/06/20

TCI Chemical

Product number: P0138
Product name: 9-Phenylanthracene
Purity: >98.0%(GC)
Packaging: 1g
Price: $113
Updated: 2024/03/01

TCI Chemical

Product number: P0138
Product name: 9-Phenylanthracene
Purity: >98.0%(GC)
Packaging: 5g
Price: $394
Updated: 2024/03/01

Alfa Aesar

Product number: H64419
Product name: 9-Phenylanthracene, 98%
Packaging: 1g
Price: $23.8
Updated: 2021/12/16

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9-phenylanthracene Chemical Properties,Usage,Production

Chemical Properties

Pale Yellow Plates

Uses

9-Phenylanthracene is used to synthesize organic light-emitting material intermediates.

Preparation

The synthesis of 9-phenylanthracene involved mixing phenylboronic acid (2.13 g, 17.49 mmol), 9-bromoanthracene (3 g, 11.66 mmol), Pd(PPh3)4 (140 mg, 0.12 mmol), K2CO3 (16 mL, 2 M), and ethanol (8 mL) in a 100 mL flask with anhydrous toluene (32 mL). The mixture was refluxed for 48 h under nitrogen. After cooled to room temperature, the reaction mixture was quenched with dilute hydrochloric acid solution and extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation. The crude product was further purified by silica gel column chromatography (CH2Cl2/petroleum ether (1:4,v/v)) to get a white powder (2.43 g, 81.9 %). 1H NMR (500 MHz, CDCl3) δ 8.53 (s, 1H), 8.08 (d, J = 8.5 Hz, 2H), 7.70 – 7.67 (m, 2H), 7.63 – 7.54 (m, 3H), 7.50 – 7.45 (m, 4H), 7.37 (ddd, J = 8.7, 6.5, 1.2 Hz, 2H). EI-MS (m/z): Calculated for C20H14: 254.33. Found [M+]: 253.02.

Synthesis of 9-phenylanthracene

Synthesis Reference(s)

Journal of the American Chemical Society, 79, p. 393, 1957 DOI: 10.1021/ja01559a042

Purification Methods

Chromatograph it on alumina in *C6H6 and recrystallise it from AcOH or toluene. [Beilstein 5 H 725, 5 II 639, 5 III 2462.]

9-phenylanthracene Preparation Products And Raw materials

Raw materials

Anthrone Bromobenzene Magnesium

Preparation Products

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View Lastest Price from 9-phenylanthracene manufacturers

WUHAN FORTUNA CHEMICAL CO., LTD

Product: 9-phenylanthracene 602-55-1
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 30tons/month
Release date: 2023-04-07

Shaanxi Dideu New Materials Co. Ltd

Product: 9-Phenylanthracene 602-55-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1000KG
Release date: 2024-11-10

Shanghai Daken Advanced Materials Co.,Ltd

Product: 9-PHENYLANTHRACENE 602-55-1
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.00%
Supply Ability: 150KG /month
Release date: 2021-11-16

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9-PHENYLANTHRACENE OEKANAL

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9-PHENYLANTHRACENE

Phenylanthracene,98%

9-PHENYLANTHRACENE OEKANAL, 250 MG

9-Phenylanthracene97%

9-Phenylanthracene 97%

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602-55-1

C6H5C14H9

C20H14

Anthracenes

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