Oxetan-3-yl Methanesulfonate

Product Name: Oxetan-3-yl Methanesulfonate
CAS No.: 148430-81-3
Chemical Name: Oxetan-3-yl Methanesulfonate
Synonyms: Oxetan-3-yl Methanesulfonate;3-Oxetanol 3-Methanesulfonate
CBNumber: CB12645851
Molecular Formula: C4H8O4S
Formula Weight: 152.17
MOL File: 148430-81-3.mol

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Oxetan-3-yl Methanesulfonate Property

Boiling point:: 308.9±31.0 °C(Predicted)
Density: 1.38±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: White to off-white Solid

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Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HS Code: 29309090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: E589565
Product name: oxetan-3-ylmethanesulfonate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 7340CZ
Product name: Oxetan-3-ylmethanesulfonate
Packaging: 250mg
Price: $134
Updated: 2021/12/16

SynQuest Laboratories

Product number: 6H64-1-09
Product name: Oxetan-3-yl methanesulfonate
Packaging: 1g
Price: $240
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0393743
Product name: OXETAN-3-YL METHANESULFONATE
Purity: 95.00%
Packaging: 5MG
Price: $495.9
Updated: 2021/12/16

Chemenu

Product number: CM200585
Product name: Oxetan-3-ylmethanesulfonate
Purity: 95%
Packaging: 5g
Price: $505
Updated: 2021/12/16

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Oxetan-3-yl Methanesulfonate Chemical Properties,Usage,Production

Synthesis

7748-36-9

124-63-0

148430-81-3

To a solution of oxetan-3-ol (5 g, 67.5 mmol) and triethylamine (14.11 mL, 101 mmol) in dichloromethane (150 mL) was added methanesulfonyl chloride (6.79 mL, 88 mmol) dropwise at 0 °C. The reaction mixture was stirred at room temperature for 3 hours. After completion of the reaction, the solid was removed by filtration and the filtrate was washed sequentially with ice water and saturated saline. The organic phase was dried with anhydrous sodium sulfate and subsequently concentrated under reduced pressure to afford oxetan-3-yl methanesulfonate (11.7 g, 67.5 mmol, 100% yield) as an oil containing 12.2 wt% dichloromethane. The product was characterized by 1H NMR (400 MHz, CDCl3): δ 3.06 (s, 3H), 4.79-4.82 (m, 2H), 4.86-4.90 (m, 2H), 5.52-5.49 (m, 1H).

References

[1] Patent: WO2013/55910, 2013, A1. Location in patent: Page/Page column 124; 125
[2] Patent: TW2017/8221, 2017, A. Location in patent: Page/Page column 98; 99
[3] Patent: WO2015/181186, 2015, A1. Location in patent: Page/Page column 169
[4] Journal of Medicinal Chemistry, 2017, vol. 60, # 23, p. 9769 - 9789
[5] Journal of Medicinal Chemistry, 2018, vol. 61, # 6, p. 2518 - 2532

Oxetan-3-yl Methanesulfonate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Oxetan-3-yl Methanesulfonate manufacturers

Career Henan Chemical Co

Product: Oxetan-3-yl Methanesulfonate 148430-81-3
Price: US $1.00/kg
Min. Order: 1kg
Purity: 95%-99%
Supply Ability: 100kg
Release date: 2018-12-22

148430-81-3, Oxetan-3-yl MethanesulfonateRelated Search:

Oxetan-3-ylhydrazine oxetane-3-sulfonamide 3-Oxetanemethanol Oxetan-3-ol methyl oxetane-3-carboxylate oxetane-3-carbaldehyde 4-Oxepanone OXETAN-3-AMINE HYDROCHLORIDE 3,3-bisz-(Hydroxymethyl)-oxetane oxepane-4-carboxylic acid 4,4,5,5-TetraMethyl-2-(oxetan-3-yl)-1,3,2-dioxaborolane AZELAICANHYDRIDE TOLUENE-4-SULFONIC ACID OXETAN-2-YLMETHYL ESTER oxetane-2-carboxylic acid methyl ester 1-(oxetan-3-yl)hydrazine dihydrochloride 2-aminomethyloxetane 1,1,1-trifluoro-3-oxetanyl Methanesulfonic acid ester 3-Oxetanemethanamine, α-phenyl-

Oxetan-3-yl Methanesulfonate

3-Oxetanol 3-Methanesulfonate

148430-81-3