6-BroMo-1-Methyl-1H-benzo[d][1,2,3]triazole
- Product Name
- 6-BroMo-1-Methyl-1H-benzo[d][1,2,3]triazole
- CAS No.
- 1083181-43-4
- Chemical Name
- 6-BroMo-1-Methyl-1H-benzo[d][1,2,3]triazole
- Synonyms
- 6-Bromo-1-methyl-1H-benzotriazole;1H-Benzotriazole, 6-bromo-1-methyl-;6-bromo-1-methyl-1H-1,2,3-benzotriazole
- CBNumber
- CB12672859
- Molecular Formula
- C7H6BrN3
- Formula Weight
- 212.05
- MOL File
- 1083181-43-4.mol
6-BroMo-1-Methyl-1H-benzo[d][1,2,3]triazole Property
- Boiling point:
- 332.6±15.0 °C(Predicted)
- Density
- 1.76±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 0.36±0.30(Predicted)
- Appearance
- Off-white to light brown Solid
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B808413
- Product name
- 6-Bromo-1-methyl-1H-benzo[d][1,2,3]triazole
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 3H32-9-DZ
- Product name
- 6-Bromo-1-methyl-1H-benzo[d][1,2,3]triazole
- Purity
- 97%
- Packaging
- 250mg
- Price
- $101
- Updated
- 2021/12/16
- Product number
- OR918875
- Product name
- 6-Bromo-1-methyl-1H-benzo[d][1,2,3]triazole
- Purity
- 97%
- Packaging
- 1g
- Price
- $153
- Updated
- 2021/12/16
- Product number
- CS-W018841
- Product name
- 6-Bromo-1-methyl-1H-benzo[d][1,2,3]triazole
- Packaging
- 1g
- Price
- $180
- Updated
- 2021/12/16
- Product number
- 119207
- Product name
- 6-Bromo-1-methyl-1H-benzo[d][1,2,3]triazole
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $216
- Updated
- 2021/12/16
6-BroMo-1-Methyl-1H-benzo[d][1,2,3]triazole Chemical Properties,Usage,Production
Synthesis
74-88-4
191230-40-7
1083181-43-4
944718-31-4
Example 2003: Compound 2003A (400 mg, 2.0 mmol) was dissolved in 10 mL of tetrahydrofuran (THF) and sodium methanolate (4 mL, 2.0 mmol) was added and reacted for 30 minutes. Subsequently, iodomethane (0.5 mL, 8.0 mmol) was added and the reaction mixture was stirred for 4 hours at room temperature. After completion of the reaction, the mixture was poured into a mixture of ethyl acetate and water. The aqueous layer was extracted twice with ethyl acetate, all organic layers were combined, washed with saturated brine solution and dried with anhydrous sodium sulfate. The solvent was removed by rotary evaporator and the product was purified by silica gel column chromatography to afford compounds 2003B (105 mg, 25% yield), 2003C (110 mg, 26% yield) and 2003D (106 mg, 25% yield), respectively.
References
[1] Patent: WO2007/84451, 2007, A1. Location in patent: Page/Page column 167
6-BroMo-1-Methyl-1H-benzo[d][1,2,3]triazole Preparation Products And Raw materials
Raw materials
Preparation Products
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