1-(3-Fluoro-pyridin-4-yl)-ethanol

Product Name: 1-(3-Fluoro-pyridin-4-yl)-ethanol
CAS No.: 87674-15-5
Chemical Name: 1-(3-Fluoro-pyridin-4-yl)-ethanol
Synonyms: 1-(3-Fluoro-pyridin-4-yl)-ethanol;4-(1-hydroxyethyl)-3-fluoropyridine;3-fluoro-a-methyl-4-Pyridinemethanol;4-Pyridinemethanol, 3-fluoro-a-methyl-;4-Pyridinemethanol, 3-fluoro-α-methyl-;3-FLUORO-ALPHA-METHYL-4-PYRIDINEMETHANOL
CBNumber: CB12727601
Molecular Formula: C7H8FNO
Formula Weight: 141.14
MOL File: 87674-15-5.mol

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1-(3-Fluoro-pyridin-4-yl)-ethanol Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
Appearance: Light brown to brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: F600180
Product name: 1-(3-Fluoropyridin-4-yl)ethanol
Packaging: 25mg
Price: $175
Updated: 2021/12/16

TRC

Product number: F600180
Product name: 1-(3-Fluoropyridin-4-yl)ethanol
Packaging: 2.5mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 4128CU
Product name: 1-(3-Fluoropyridin-4-yl)ethanol
Packaging: 100mg
Price: $85
Updated: 2021/12/16

Ambeed

Product number: A312744
Product name: 1-(3-Fluoropyridin-4-yl)ethanol
Purity: 95+%
Packaging: 1g
Price: $109
Updated: 2021/12/16

Chemenu

Product number: CM255505
Product name: 1-(3-Fluoropyridin-4-yl)ethanol
Purity: 95%
Packaging: 1g
Price: $137
Updated: 2021/12/16

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1-(3-Fluoro-pyridin-4-yl)-ethanol Chemical Properties,Usage,Production

Synthesis

372-47-4

75-07-0

87674-15-5

To a stirred solution of 3-fluoropyridine (14 g, 144.2 mmol) in anhydrous THF (150 mL), cooled to -78°C under argon protection, a n-heptane/THF/ethylbenzene solution (79.2 mL, 158.6 mmol) of lithium 2 N diisopropylammonium (LDA) was added slowly dropwise over a period of about 1 hour. After stirring for 2.5 hours, a solution of acetaldehyde (8.9 mL, 158.5 mmol) in 25 mL of anhydrous THF cooled to about 0°C was added slowly dropwise and the reaction mixture was continued to be stirred at -78°C for 1.5 hours. Subsequently, the reaction solution was slowly warmed to -30 °C and the reaction was quenched by the addition of a solution of ammonium chloride (150 g) in 700 mL of water. The mixture was extracted with ethyl acetate (3 x 400 mL) and the combined organic layers were washed with brine (4 x 200 mL) and dried over anhydrous sodium sulfate. After concentrating the organic phase, the residual oily material was crystallized with hexane (40 mL) to give 15.6 g (76% yield) of 1-(3-fluoropyridin-4-yl)ethanol.

References

[1] Patent: WO2005/13986, 2005, A1. Location in patent: Page/Page column 44
[2] Patent: US2007/142414, 2007, A1. Location in patent: Page/Page column 18-19
[3] Patent: WO2007/96334, 2007, A1. Location in patent: Page/Page column 31-32
[4] Tetrahedron, 1983, vol. 39, # 12, p. 2009 - 2021

1-(3-Fluoro-pyridin-4-yl)-ethanol Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(3-Fluoro-pyridin-4-yl)-ethanol Suppliers

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View Lastest Price from 1-(3-Fluoro-pyridin-4-yl)-ethanol manufacturers

Career Henan Chemical Co

Product: 4-(1-hydroxyethyl)-3-fluoropyridine 87674-15-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: Min98% HPLC
Supply Ability: g/kg/ton
Release date: 2020-02-05

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87674-15-5