1-BROMO-4-DECYLBENZENE
- Product Name
- 1-BROMO-4-DECYLBENZENE
- CAS No.
- 106418-67-1
- Chemical Name
- 1-BROMO-4-DECYLBENZENE
- Synonyms
- 88.0%(GC);4-DECYLBROMOBENZENE;4-N-DECYLBROMOBENZENE;1-BROMO-4-DECYLBENZENE;4-Decyl-1-bromobenzene;4-Bromo-1-decylbenzene;1-BROMO-4-N-DECYLBENZENE;Benzene,1-bromo-4-decyl-;1-Bromo-4-decylbenzene >
- CBNumber
- CB1310133
- Molecular Formula
- C16H25Br
- Formula Weight
- 297.27
- MOL File
- 106418-67-1.mol
1-BROMO-4-DECYLBENZENE Property
- Boiling point:
- 346℃
- Density
- 1.099
- Flash point:
- 206℃
- refractive index
- 1.5110
- storage temp.
- Sealed in dry,Room Temperature
- form
- Liquid
- color
- Colorless to pale yellow
- InChI
- InChI=1S/C16H25Br/c1-2-3-4-5-6-7-8-9-10-15-11-13-16(17)14-12-15/h11-14H,2-10H2,1H3
- InChIKey
- SWTGVSCSSDYINB-UHFFFAOYSA-N
- SMILES
- C1(Br)=CC=C(CCCCCCCCCC)C=C1
- CAS DataBase Reference
- 106418-67-1
Safety
- HS Code
- 2903.99.8001
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B1611
- Product name
- 1-Bromo-4-decylbenzene
- Purity
- >88.0%(GC)
- Packaging
- 1g
- Price
- $47
- Updated
- 2025/07/31
- Product number
- B1611
- Product name
- 1-Bromo-4-decylbenzene
- Purity
- >88.0%(GC)
- Packaging
- 5g
- Price
- $147
- Updated
- 2025/07/31
- Product number
- B1611
- Product name
- 1-Bromo-4-decylbenzene
- Purity
- >88.0%(GC)
- Packaging
- 25g
- Price
- $500
- Updated
- 2025/07/31
- Product number
- B677885
- Product name
- 1-Bromo-4-decylbenzene
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B677885
- Product name
- 1-Bromo-4-decylbenzene
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
1-BROMO-4-DECYLBENZENE Chemical Properties,Usage,Production
Synthesis
134443-99-5
106418-67-1
1-Bromo-4-decylbenzene was synthesized by the Wolff-Kishner reaction using 1-(4-bromophenyl)decan-1-one 7 (1.3 g, 4.2 mmol) as raw material. The procedure was as follows: 1-(4-bromophenyl)decan-1-one 7, hydrazine monohydrate (1.2 mL, 16 mmol) and KOH (1.8 g, 32 mmol) were dissolved in 25 mL of 1-octanol in a 50 mL two-neck flask to form a green suspension. The reaction mixture was stirred at reflux for 2 h at 135 °C until the solution was almost colorless. After completion of the reaction, the mixture was cooled to room temperature, diluted with ether (50 mL) and washed sequentially with aqueous 1N HCl (50 mL), aqueous 2N HCl (20 mL) and brine (2 x 30 mL). The organic phase was dried over MgSO4, filtered and concentrated in vacuum. 1-Octanol was removed by vacuum distillation to give about 2.7 g of crude product. The crude product was purified by column chromatography using heptane as eluent to give a final colorless oily product in 40% yield. The product was detected by TLC (Rf = 0.61, 100% heptane).1H NMR (500 MHz, CDCl3) δ 7.37 (d, J = 8.3Hz, 2H), 7.03 (d, J = 8.1Hz, 2H), 2.54 (t, J = 7.7Hz, 2H), 1.60-1.54 (m, 2H), 1.28-1.25 (m, 2H). 14H), 0.88 (t, J = 6.8 Hz, 3H).13C NMR (50 MHz, CDCl3) δ 142.05, 131.46, 130.37, 119.47, 35.59, 32.14, 31.56, 29.85, 29.82, 29.71, 29.57, 29.43, 22.93. 14.34. ms (APPI): m/z 296.2 [M+].
References
[1] Macromolecules, 2010, vol. 43, # 19, p. 8063 - 8070
[2] Bulletin of the Korean Chemical Society, 2012, vol. 33, # 2, p. 541 - 548
[3] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 24, p. 7763 - 7778
[4] Journal of Materials Chemistry, 2003, vol. 13, # 1, p. 50 - 55
[5] Molecular Crystals and Liquid Crystals, 2003, vol. 396, p. 241 - 250
1-BROMO-4-DECYLBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 1-BROMO-4-DECYLBENZENE manufacturers
- Product
- 1-BROMO-4-DECYLBENZENE 106418-67-1
- Price
- US $101.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-28
- Product
- 1-Bromo-4-decylbenzene 106418-67-1
- Price
- US $9.80/KG
- Min. Order
- 1KG
- Purity
- >98%HPLC
- Supply Ability
- 20 tons
- Release date
- 2020-02-06