ChemicalBook > CAS DataBase List > 1-BROMO-4-DECYLBENZENE

1-BROMO-4-DECYLBENZENE

Product Name
1-BROMO-4-DECYLBENZENE
CAS No.
106418-67-1
Chemical Name
1-BROMO-4-DECYLBENZENE
Synonyms
88.0%(GC);4-DECYLBROMOBENZENE;4-N-DECYLBROMOBENZENE;1-BROMO-4-DECYLBENZENE;4-Decyl-1-bromobenzene;4-Bromo-1-decylbenzene;1-BROMO-4-N-DECYLBENZENE;Benzene,1-bromo-4-decyl-;1-Bromo-4-decylbenzene >
CBNumber
CB1310133
Molecular Formula
C16H25Br
Formula Weight
297.27
MOL File
106418-67-1.mol
More
Less

1-BROMO-4-DECYLBENZENE Property

Boiling point:
346℃
Density 
1.099
Flash point:
206℃
refractive index 
1.5110
storage temp. 
Sealed in dry,Room Temperature
form 
Liquid
color 
Colorless to pale yellow
InChI
InChI=1S/C16H25Br/c1-2-3-4-5-6-7-8-9-10-15-11-13-16(17)14-12-15/h11-14H,2-10H2,1H3
InChIKey
SWTGVSCSSDYINB-UHFFFAOYSA-N
SMILES
C1(Br)=CC=C(CCCCCCCCCC)C=C1
CAS DataBase Reference
106418-67-1
More
Less

Safety

HS Code 
2903.99.8001
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More
Less

N-Bromosuccinimide Price

TCI Chemical
Product number
B1611
Product name
1-Bromo-4-decylbenzene
Purity
>88.0%(GC)
Packaging
1g
Price
$47
Updated
2025/07/31
TCI Chemical
Product number
B1611
Product name
1-Bromo-4-decylbenzene
Purity
>88.0%(GC)
Packaging
5g
Price
$147
Updated
2025/07/31
TCI Chemical
Product number
B1611
Product name
1-Bromo-4-decylbenzene
Purity
>88.0%(GC)
Packaging
25g
Price
$500
Updated
2025/07/31
TRC
Product number
B677885
Product name
1-Bromo-4-decylbenzene
Packaging
50mg
Price
$45
Updated
2021/12/16
TRC
Product number
B677885
Product name
1-Bromo-4-decylbenzene
Packaging
500mg
Price
$110
Updated
2021/12/16
More
Less

1-BROMO-4-DECYLBENZENE Chemical Properties,Usage,Production

Synthesis

134443-99-5

106418-67-1

1-Bromo-4-decylbenzene was synthesized by the Wolff-Kishner reaction using 1-(4-bromophenyl)decan-1-one 7 (1.3 g, 4.2 mmol) as raw material. The procedure was as follows: 1-(4-bromophenyl)decan-1-one 7, hydrazine monohydrate (1.2 mL, 16 mmol) and KOH (1.8 g, 32 mmol) were dissolved in 25 mL of 1-octanol in a 50 mL two-neck flask to form a green suspension. The reaction mixture was stirred at reflux for 2 h at 135 °C until the solution was almost colorless. After completion of the reaction, the mixture was cooled to room temperature, diluted with ether (50 mL) and washed sequentially with aqueous 1N HCl (50 mL), aqueous 2N HCl (20 mL) and brine (2 x 30 mL). The organic phase was dried over MgSO4, filtered and concentrated in vacuum. 1-Octanol was removed by vacuum distillation to give about 2.7 g of crude product. The crude product was purified by column chromatography using heptane as eluent to give a final colorless oily product in 40% yield. The product was detected by TLC (Rf = 0.61, 100% heptane).1H NMR (500 MHz, CDCl3) δ 7.37 (d, J = 8.3Hz, 2H), 7.03 (d, J = 8.1Hz, 2H), 2.54 (t, J = 7.7Hz, 2H), 1.60-1.54 (m, 2H), 1.28-1.25 (m, 2H). 14H), 0.88 (t, J = 6.8 Hz, 3H).13C NMR (50 MHz, CDCl3) δ 142.05, 131.46, 130.37, 119.47, 35.59, 32.14, 31.56, 29.85, 29.82, 29.71, 29.57, 29.43, 22.93. 14.34. ms (APPI): m/z 296.2 [M+].

References

[1] Macromolecules, 2010, vol. 43, # 19, p. 8063 - 8070
[2] Bulletin of the Korean Chemical Society, 2012, vol. 33, # 2, p. 541 - 548
[3] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 24, p. 7763 - 7778
[4] Journal of Materials Chemistry, 2003, vol. 13, # 1, p. 50 - 55
[5] Molecular Crystals and Liquid Crystals, 2003, vol. 396, p. 241 - 250

1-BROMO-4-DECYLBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

1-BROMO-4-DECYLBENZENE Suppliers

TCI AMERICA
Tel
800-4238616
Fax
+1-888-520-1075 / +1-503-283-1987
Email
sales@tciamerica.com
Country
Americas
ProdList
23653
Advantage
75
More
Less

View Lastest Price from 1-BROMO-4-DECYLBENZENE manufacturers

Henan Fengda Chemical Co., Ltd
Product
1-BROMO-4-DECYLBENZENE 106418-67-1
Price
US $101.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-28
Career Henan Chemical Co
Product
1-Bromo-4-decylbenzene 106418-67-1
Price
US $9.80/KG
Min. Order
1KG
Purity
>98%HPLC
Supply Ability
20 tons
Release date
2020-02-06

106418-67-1, 1-BROMO-4-DECYLBENZENERelated Search:


  • 4-DECYLBROMOBENZENE
  • 4-N-DECYLBROMOBENZENE
  • 1-BROMO-4-DECYLBENZENE
  • 1-BROMO-4-N-DECYLBENZENE
  • 4-Bromo-1-decylbenzene
  • 4-Decyl-1-bromobenzene
  • Benzene,1-bromo-4-decyl-
  • 1-Bromo-4-decylbenzene &gt
  • 88.0%(GC)
  • 106418-67-1
  • 4-Alkylbromobenzenes (Building Blocks for Liquid Crystals)
  • Building Blocks for Liquid Crystals
  • 4-Alkylbromobenzenes (Building Blocks for Liquid Crystals)
  • Building Blocks for Liquid Crystals
  • Functional Materials