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DIENESTROL

Product Name
DIENESTROL
CAS No.
84-17-3
Chemical Name
DIENESTROL
Synonyms
DV;Agaldog;Restrol;Retalon;Dinovex;Estroral;Oestrora;Sexadien;Teserene;para-Dien
CBNumber
CB1312612
Molecular Formula
C18H18O2
Formula Weight
266.33
MOL File
84-17-3.mol
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DIENESTROL Property

Melting point:
229 °C
Boiling point:
349.54°C (rough estimate)
Density 
1.184 g/cm3
refractive index 
1.4800 (estimate)
storage temp. 
Sealed in dry,Room Temperature
solubility 
DMSO (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
form 
Solid
pka
9.21±0.15(Predicted)
color 
Pale Yellow to Pale Beige
Water Solubility 
3mg/L(37 ºC)
Merck 
3104
BRN 
2053694
CAS DataBase Reference
84-17-3
EPA Substance Registry System
Dienestrol (84-17-3)
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Safety

Hazard Codes 
Xn,T
Risk Statements 
40-48-62-45
Safety Statements 
22-24/25-45-36/37-53
WGK Germany 
3
RTECS 
SL0580000
HS Code 
2907.29.0500
Hazardous Substances Data
84-17-3(Hazardous Substances Data)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H350May cause cancer

Precautionary statements

P201Obtain special instructions before use.

P202Do not handle until all safety precautions have been read and understood.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P308+P313IF exposed or concerned: Get medical advice/attention.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
D1200000
Product name
Dienestrol
Purity
European Pharmacopoeia (EP) Reference Standard
Packaging
d1200000
Price
$150
Updated
2024/03/01
TCI Chemical
Product number
D0449
Product name
Dienestrol
Purity
>96.0%(GC)
Packaging
1g
Price
$128
Updated
2021/12/16
TCI Chemical
Product number
D0449
Product name
Dienestrol
Purity
>96.0%(GC)
Packaging
100mg
Price
$22
Updated
2024/03/01
Usbiological
Product number
D3550-01C
Product name
Dienestrol
Packaging
500ul
Price
$393
Updated
2021/12/16
TRC
Product number
D441805
Product name
Dienestrol
Packaging
2.5g
Price
$545
Updated
2021/12/16
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DIENESTROL Chemical Properties,Usage,Production

Chemical Properties

Colorless, needles or powder; odorless. Soluble in alcohol; practically insoluble in water; sensitive to light.

Originator

Synestrol,Schering,US,1947

Uses

Dienestrol is a metabolite of Diethylstilbestrol, a non-steroidal synthetic estrogen derivative.

Uses

Medicine (estrogenic hormone).

Definition

ChEBI: An olefinic compound that is hexa-2,4-diene substituted by 4-hydroxyphenyl groups at positions 3 and 4 respectively.

Manufacturing Process

Preparation of γ,δ-Bis-(4-Hydroxylphenyl)-Hexane-γ,δ-Diol: A sodium amalgam is prepared containing 6 grams of sodium and 400 grams of mercury. The amalgam is covered with a solution of 20 grams of 4-hydroxypropiophenone in a mixture of 30 ml of 5 N sodium hydroxide solution and 220 ml of water and the mixture is heated to 28°-30°C and stirred gently. The reduction is accompanied by development of heat and the temperature of the solution rises to 34°-35°C, and then falls slowly. After 5 hours the alkaline solution is separated from the mercury and diluted with 3 or 4 times its volume of water, when, in order to form the benzoyl derivatives of the products, the solution is vigorously stirred, while it is being cooled, with 20 ml of benzoyl chloride, the solution being kept at a temperature of 15°-20°C. When the reaction is completed, the benzoyl derivatives are filtered off, washed with water and recrystallized from a mixture of benzene and alcohol, when a product with a melting point of 195°-215°C is obtained.
Preparation of Dienestrol: In order to obtain dienoestrol, 14.6 grams of dry 4,4'-dibenzoate are refluxed with a mixture of 40 ml of acetic anhydride and 40 ml acetylchloride by heating in an oil-bath at about 90°C for 6 hours after which the bath temperature is increased to 120°C and heating continued for a further 18 hours, after which time the evolution of hydrogen chloride practically ceases. The mixture is allowed to cool for several hours and the crystals which separate are filtered off and recrystallized from an alcoholbenzene mixture when the product melts at 210°-222°C. This product is converted into dienoestrol by adding 10.8 grams of it to 100 ml of 10% (w/v) alcoholic potassium hydroxide solution and then refluxing during 1 hour. After dilution with 200 ml of water and filtration from a small amount of insoluble material, dienoestrol is precipitated from the alkaline solution by treatment with carbon dioxide. It is filtered off, washed with water and recrystallized from dilute alcohol after which it melts at 233°-234°C according to US Patent 2,464,203.

brand name

Avc/dienestrol;Crinohermal fem;D.v.;Dienostrol cream;Dienstrogen;Dinol;Dufemine;Foragynol;Frein;Klianyi forte;Klianyl;Neo-oestrogenine;Ortho (cream);Ortho dienestrol cream.

Therapeutic Function

Estrogen

World Health Organization (WHO)

Dienestrol is a stilbene derivative. See WHO comment for diethylstilbestrol. Vaginal forms of dienestrol, which were introduced in 1947, are currently available in over 35 countries for the management of hypoestrogenic vaginal atrophy. (Reference: (WHODI) WHO Drug Information, 77.1, 16, 1977)

Safety Profile

Suspected human carcinogen. Human mutation data reported. Experimental reproductive effects. Used as a drug for the treatment of postmenopausal symptoms. When heated to decomposition it emits acrid smoke and irritating fumes.

DIENESTROL Preparation Products And Raw materials

Raw materials

Preparation Products

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DIENESTROL Suppliers

J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
Advantage
76
Meryer (Shanghai) Chemical Technology Co., Ltd.
Tel
021-61259108 18621169109
Fax
86-21-61259102
Email
market03@meryer.com
Country
China
ProdList
40228
Advantage
62
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
Advantage
81
Energy Chemical
Tel
021-021-58432009 400-005-6266
Fax
021-58436166
Email
sales8178@energy-chemical.com
Country
China
ProdList
44688
Advantage
61
Nanjing Chemlin Chemical Co., Ltd
Tel
025-83697070
Fax
+86-25-83453306
Email
info@chemlin.com.cn
Country
China
ProdList
19179
Advantage
64
Shandong Xiya Chemical Co., Ltd
Tel
4009903999 13355009207
Fax
0539-6365991
Email
3007715519@qq.com
Country
China
ProdList
18738
Advantage
57
Sichuan Kulinan Technology Co., Ltd
Tel
400-1166-196 18981987031
Fax
028-84555506 800101999
Email
cdhxsj@163.com
Country
China
ProdList
11707
Advantage
57
Sinopharm Chemical Reagent Co,Ltd.
Tel
86-21-63210123
Fax
86-21-63290778 86-21-63218885
Email
sj_scrc@sinopharm.com
Country
China
ProdList
9815
Advantage
79
Maya High Purity Chemicals
Tel
+86 (573) 82222445 (0)18006601000 452520369
Fax
+86 (573) 82222643
Email
sales@maya-r.com
Country
China
ProdList
11707
Advantage
57
Chengdu Ai Keda Chemical Technology Co., Ltd.
Tel
4008-755-333 18080918076
Fax
028-86757656
Email
800078821@qq.com
Country
China
ProdList
9718
Advantage
55
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View Lastest Price from DIENESTROL manufacturers

Career Henan Chemical Co
Product
DIENESTROL 84-17-3
Price
US $1.00/KG
Min. Order
1KG
Purity
95-99%
Supply Ability
1ton
Release date
2020-01-03

84-17-3, DIENESTROLRelated Search:


  • 4,4’-hydroxy-gamma,delta-diphenyl-beta,delta-hexadiene
  • 4,4'-Hydroxy-gamma,delta-diphenyl-beta,delta-hexadiene
  • Agaldog
  • 3,4-bis(4-hydroxyphenyl)-4-hexadiene
  • 3,4-bis(para-hydroxyphenyl)-2,4-hexadiene
  • 4,4'-(1,2-Diethylidene-1,2-ethanediyl)bisphenol
  • 4,4’-(1,2-diethylidene-1,2-ethanediyl)bis-pheno
  • 4,4’-(1,2-diethylidene-1,2-ethanediyl)bisphenol
  • 4,4’-(diethylideneethylene)di-pheno
  • para,para’-(diethylideneethylene)diphenol
  • para-Dien
  • Phenol, 4,4'-(1,2-diethylidene-1,2-ethanediyl)bis-
  • Phenol, 4,4'-(1,2-diethylidene-1,2-ethanediyl)bis-, (E,E)-
  • Phenol, 4,4'-(diethylideneethylene)di-
  • Restrol
  • Retalon
  • 3,4-BIS(4-HYDROXYPHENYL)-2,4-HEXADIENE
  • 3 4-BIS(P-HYDROXYPHENYL)-2 4-HEXADIENE
  • 3,4-DI(P-OXYPHENYL)-2 4-HEXADIENE
  • 4,4'-DIHYDROXY-GAMMA,DELTA-DIPHENYL-BETA,DELTA-HEXADIENE
  • 4,4'-(DIETHYLIDENEETHYLENE)DIPHENOL
  • DIENESTROL
  • CYCLADIENE
  • beta-Dienoestrol
  • Dehydrostilbestrol
  • Dehydrostilboestrol
  • di(para-oxyphenyl)-2,4-hexadiene
  • Di(p-oxyphenyl)-2,4-hexadiene
  • Dienesterol
  • Dienoestrol
  • Dienoestrol bp
  • Dinestrol
  • Dinovex
  • DV
  • Estragard
  • Estraguard
  • Estrodienol
  • Estroral
  • Follormon
  • Gynefollin
  • Hormofemin
  • Oestrasid
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  • Oestrodienol
  • Oestroral
  • Oestrovis
  • p,p'-(Diethylideneethylene)diphenol
  • p,p’-(diethylideneethylene)diphenol
  • Dienestrol (125 mg)
  • 4,4′-Dihydroxy-γ,δ-diphenyl-β,δ-hexadiene
  • Oestrora
  • Dienestrol Solution, 100ppm
  • 2,4-Hexadiene, 3,4-bis(4-hydroxyphenyl)-
  • Sexadien
  • Teserene
  • Willnestrol
  • DIENESTROL VETRANAL, 250 MG
  • DIENESTROL CRYSTALLINE