3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole

Product Name: 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
CAS No.: 1309788-50-8
Chemical Name: 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
Synonyms: 3-iodo-6,6-dimethyl-1,4,5,7-tetrahydroindazole;3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole;1H-Indazole, 4,5,6,7-tetrahydro-3-iodo-6,6-dimethyl-
CBNumber: CB13374659
Molecular Formula: C9H13IN2
Formula Weight: 276.12
MOL File: 1309788-50-8.mol

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3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Property

Boiling point:: 360.1±42.0 °C(Predicted)
Density: 1.640±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 12.56±0.40(Predicted)
Appearance: Off-white to yellow Solid
InChI: InChI=1S/C9H13IN2/c1-9(2)4-3-6-7(5-9)11-12-8(6)10/h3-5H2,1-2H3,(H,11,12)
InChIKey: ZDWZKCXTTCFVQE-UHFFFAOYSA-N
SMILES: N1C2=C(CCC(C)(C)C2)C(I)=N1

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific

Product number: 1117DP
Product name: 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
Packaging: 100mg
Price: $118
Updated: 2021/12/16

Chemenu

Product number: CM231817
Product name: 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
Purity: 95+%
Packaging: 250mg
Price: $154
Updated: 2021/12/16

Ambeed

Product number: A312056
Product name: 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
Purity: 97%
Packaging: 1g
Price: $176
Updated: 2021/12/16

Acrotein

Product number: UT00365
Product name: 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
Purity: 97%
Packaging: 0.25g
Price: $258.33
Updated: 2021/12/16

Crysdot

Product number: CD11297095
Product name: 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
Purity: 97%
Packaging: 250mg
Price: $284
Updated: 2021/12/16

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3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Chemical Properties,Usage,Production

Synthesis

1309788-49-5

1309788-50-8

Step 3: 6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole (0.50 g, 3.33 mmol) was dissolved in DMF (8 mL) at room temperature and powdered potassium hydroxide (560 mg, 10.0 mmol) and iodine (1.69 g, 6.66 mmol) were added sequentially. The reaction mixture was stirred for 45 min until the color changed to maroon. Upon completion of the reaction, the reaction was quenched with 10% Na2S2O3 aqueous solution, diluted with water and extracted with EtOAc (2×). The organic phases were combined, washed with water (3×), dried over MgSO4 and concentrated to give 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole (920 mg, 99% yield) as a pale yellow waxy solid.1H NMR (CDCl3, 300 MHz) δ (ppm): 2.44 (s, 2H), 2.35 (t, J = 6.4 Hz, 2H), 1.55 (t, J = 6.4 Hz, 2H), 1.01 (s, 6H).

References

[1] Patent: WO2013/30138, 2013, A1. Location in patent: Page/Page column 196
[2] Patent: US2011/306599, 2011, A1. Location in patent: Page/Page column 32; 33
[3] Patent: WO2014/41518, 2014, A1. Location in patent: Page/Page column 37

3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Preparation Products And Raw materials

Raw materials

Preparation Products

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3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Suppliers

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View Lastest Price from 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole 1309788-50-8
Price: US $2.00-6.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-08-06

1309788-50-8, 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazoleRelated Search:

3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole

1H-Indazole, 4,5,6,7-tetrahydro-3-iodo-6,6-dimethyl-

3-iodo-6,6-dimethyl-1,4,5,7-tetrahydroindazole

1309788-50-8