3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- Product Name
- 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- CAS No.
- 1309788-50-8
- Chemical Name
- 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- Synonyms
- 3-iodo-6,6-dimethyl-1,4,5,7-tetrahydroindazole;3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole;1H-Indazole, 4,5,6,7-tetrahydro-3-iodo-6,6-dimethyl-
- CBNumber
- CB13374659
- Molecular Formula
- C9H13IN2
- Formula Weight
- 276.12
- MOL File
- 1309788-50-8.mol
3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Property
- Boiling point:
- 360.1±42.0 °C(Predicted)
- Density
- 1.640±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 12.56±0.40(Predicted)
- Appearance
- Off-white to yellow Solid
- InChI
- InChI=1S/C9H13IN2/c1-9(2)4-3-6-7(5-9)11-12-8(6)10/h3-5H2,1-2H3,(H,11,12)
- InChIKey
- ZDWZKCXTTCFVQE-UHFFFAOYSA-N
- SMILES
- N1C2=C(CCC(C)(C)C2)C(I)=N1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 1117DP
- Product name
- 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- Packaging
- 100mg
- Price
- $118
- Updated
- 2021/12/16
- Product number
- CM231817
- Product name
- 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $154
- Updated
- 2021/12/16
- Product number
- A312056
- Product name
- 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- Purity
- 97%
- Packaging
- 1g
- Price
- $176
- Updated
- 2021/12/16
- Product number
- UT00365
- Product name
- 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- Purity
- 97%
- Packaging
- 0.25g
- Price
- $258.33
- Updated
- 2021/12/16
- Product number
- CD11297095
- Product name
- 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole
- Purity
- 97%
- Packaging
- 250mg
- Price
- $284
- Updated
- 2021/12/16
3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Chemical Properties,Usage,Production
Synthesis
1309788-49-5
1309788-50-8
Step 3: 6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole (0.50 g, 3.33 mmol) was dissolved in DMF (8 mL) at room temperature and powdered potassium hydroxide (560 mg, 10.0 mmol) and iodine (1.69 g, 6.66 mmol) were added sequentially. The reaction mixture was stirred for 45 min until the color changed to maroon. Upon completion of the reaction, the reaction was quenched with 10% Na2S2O3 aqueous solution, diluted with water and extracted with EtOAc (2×). The organic phases were combined, washed with water (3×), dried over MgSO4 and concentrated to give 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole (920 mg, 99% yield) as a pale yellow waxy solid.1H NMR (CDCl3, 300 MHz) δ (ppm): 2.44 (s, 2H), 2.35 (t, J = 6.4 Hz, 2H), 1.55 (t, J = 6.4 Hz, 2H), 1.01 (s, 6H).
References
[1] Patent: WO2013/30138, 2013, A1. Location in patent: Page/Page column 196
[2] Patent: US2011/306599, 2011, A1. Location in patent: Page/Page column 32; 33
[3] Patent: WO2014/41518, 2014, A1. Location in patent: Page/Page column 37
3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Preparation Products And Raw materials
Raw materials
Preparation Products
3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole Suppliers
- Tel
- --
- Fax
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- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
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View Lastest Price from 3-iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole manufacturers
- Product
- 3-Iodo-6,6-dimethyl-4,5,6,7-tetrahydro-1H-indazole 1309788-50-8
- Price
- US $2.00-6.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2025-08-06