ChemicalBook > CAS DataBase List > 3-Benzyl-3,7-diazabicyclo[3.3.0]octane

3-Benzyl-3,7-diazabicyclo[3.3.0]octane

Product Name: 3-Benzyl-3,7-diazabicyclo[3.3.0]octane
CAS No.: 86732-22-1
Chemical Name: 3-Benzyl-3,7-diazabicyclo[3.3.0]octane
Synonyms: 4,5-DIHYDROBENZO[D...;3-Benzyl-3,7-diazabicyclo[3.3.0]octane;Octahydro-2-benzylpyrrolo[3,4-c]pyrrole;2-BENZYL-OCTAHYDRO-PYRROLO [3,4-C] PYRROLE;3-BENZYL-3,7-DIAZABICYCLO[3.3.0]OCTANE,98%;2-Benzyl-Octahydro-Pyrrolo[3,4-C]Pyrrole HCl;Pyrrolo[3,4-c]pyrrole, octahydro-2-(phenylmethyl)-;5-(phenylmethyl)-2,3,3a,4,6,6a-hexahydro-1H-pyrrolo[3,4-c]pyrrole
CBNumber: CB1337941
Molecular Formula: C13H18N2
Formula Weight: 202.3
MOL File: 86732-22-1.mol

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3-Benzyl-3,7-diazabicyclo[3.3.0]octane Property

storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: Colorless to light yellow Liquid

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Safety

Hazard Codes: Xn
Risk Statements: 22
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B130090
Product name: 2-Benzyloctahydropyrrolo[3,4-C]Pyrrole
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB51190
Product name: 2-Benzyl-octahydro-pyrrolo [3,4-c] pyrrole
Packaging: 50mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB51190
Product name: 2-Benzyl-octahydro-pyrrolo [3,4-c] pyrrole
Packaging: 100mg
Price: $104
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB51190
Product name: 2-Benzyl-octahydro-pyrrolo [3,4-c] pyrrole
Packaging: 250mg
Price: $130
Updated: 2021/12/16

Apolloscientific

Product number: OR931334
Product name: 2-Benzyloctahydropyrrolo[3,4-c]pyrrole
Purity: >98%
Packaging: 1g
Price: $179
Updated: 2021/12/16

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3-Benzyl-3,7-diazabicyclo[3.3.0]octane Chemical Properties,Usage,Production

Synthesis

848591-86-6

86732-22-1

The general procedure for the synthesis of 3-benzyl-3,7-diazabicyclo[3.3.0]octane from the compound (CAS:848591-86-6) was as follows: first, 5-benzyltetrahydropyrrolo[3,4-c]pyrrole-1,3-dione (4.9 g, 0.021 mol) was dissolved in pre-cooled to 0 °C anhydrous tetrahydrofuran (THF) under nitrogen protection ( 50 mL). Subsequently, a THF solution of lithium aluminum hydride (63 mL, 1 M, 0.063 mol) was slowly added dropwise over 30 min while keeping the reaction mixture at 0 °C. After the dropwise addition was completed, the reaction mixture was stirred at room temperature for 30 minutes and then heated to reflux for 4 hours. Upon completion of the reaction, the mixture was cooled to 0 °C and the reaction was quenched by slow addition of excess sodium sulfate decahydrate solid. The mixture was returned to room temperature and stirring was continued for 16 hours. The solid was removed by filtration and the filtrate was washed with ethyl acetate (3 x 100 mL). The filtrates were combined and concentrated to give 4.2 g (99% yield) of the waxy solid product, which was analyzed by mass spectrometry to show m/z 203 (M + H).

References

[1] Patent: WO2008/57938, 2008, A1. Location in patent: Page/Page column 30
[2] Patent: WO2006/12396, 2006, A1. Location in patent: Page/Page column 21; 34
[3] Patent: WO2013/71697, 2013, A1. Location in patent: Paragraph 00248
[4] Patent: US2014/228361, 2014, A1. Location in patent: Paragraph 0368-0369
[5] Patent: US2005/101602, 2005, A1. Location in patent: Page/Page column 28

3-Benzyl-3,7-diazabicyclo[3.3.0]octane Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Benzyl-3,7-diazabicyclo[3.3.0]octane Suppliers

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View Lastest Price from 3-Benzyl-3,7-diazabicyclo[3.3.0]octane manufacturers

Career Henan Chemical Co

Product: 3-Benzyl-3,7-diazabicyclo[3.3.0]octane 86732-22-1
Price: US $1.00/kg
Min. Order: 1g
Purity: 99%
Supply Ability: 100KG
Release date: 2018-12-21

86732-22-1, 3-Benzyl-3,7-diazabicyclo[3.3.0]octaneRelated Search:

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4,5-DIHYDROBENZO[D...

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86732-22-1

Heterocycles series

Amines and Anilines