ChemicalBook > CAS DataBase List > 4-BROMO-6-METHOXYINDOLE

4-BROMO-6-METHOXYINDOLE

Product Name: 4-BROMO-6-METHOXYINDOLE
CAS No.: 393553-55-4
Chemical Name: 4-BROMO-6-METHOXYINDOLE
Synonyms: 4-BROMO-6-METHOXYINDOLE;4-BROMO-6-METHYLOXY INDOLE;4-bromo-6-methoxy-1H-indole;4-broMo-6-Methyloxyl indole;1H-Indole, 4-broMo-6-Methoxy-
CBNumber: CB1348446
Molecular Formula: C9H8BrNO
Formula Weight: 226.07
MOL File: 393553-55-4.mol

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4-BROMO-6-METHOXYINDOLE Property

Boiling point:: 346.8±22.0 °C(Predicted)
Density: 1.591±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 16.29±0.30(Predicted)
Appearance: Off-white to light brown Solid
InChI: InChI=1S/C9H8BrNO/c1-12-6-4-8(10)7-2-3-11-9(7)5-6/h2-5,11H,1H3
InChIKey: CZJYKEPYJHPVOD-UHFFFAOYSA-N
SMILES: N1C2=C(C(Br)=CC(OC)=C2)C=C1

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B429763
Product name: 4-bromo-6-methoxy-1H-indole
Packaging: 1mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B429763
Product name: 4-bromo-6-methoxy-1H-indole
Packaging: 2mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0320033
Product name: 4-BROMO-6-METHOXYINDOLE
Purity: 95.00%
Packaging: 5MG
Price: $497.1
Updated: 2021/12/16

AK Scientific

Product number: 5147AB
Product name: 4-Bromo-6-methoxy-1H-indole
Packaging: 5g
Price: $1308
Updated: 2021/12/16

Ambeed

Product number: A171194
Product name: 4-Bromo-6-methoxy-1H-indole
Purity: 98%
Packaging: 100mg
Price: $74
Updated: 2021/12/16

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4-BROMO-6-METHOXYINDOLE Chemical Properties,Usage,Production

Synthesis

1431711-54-4

393553-55-4

General procedure for the synthesis of 4-bromo-6-methoxy-1H-indole from the compound (CAS: 1431711-54-4): (b) N-(3-bromo-5-methoxyphenyl)-N-hydroxyacetamide (360 mg, 1.384 mmol) was dissolved in vinyl acetate (1.92 mL) followed by addition of Li2PdCl4 (18.2 mg, 69 μmol). The reaction mixture was stirred at 60°C for 3 hours. After completion of the reaction, the reaction mixture was diluted with ethyl acetate (EtOAc) and brine, the organic layer was separated and concentrated under reduced pressure to give a solid. The solid was dissolved in methanol (20 mL), 1N NaOH aqueous solution (2.61 mL, 2.61 mmol) was added and stirred for 2 hours at room temperature. The reaction mixture was quenched with 2N HCl aqueous solution (1.3 mL, 2.6 mmol) followed by addition of sodium carbonate (500 mg). After addition of ethyl acetate (50 mL), the organic layer was separated, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated. The residue was purified by column chromatography (20 g silica gel, ethyl acetate/heptane, gradient from 0/100 to 1/4) to afford the title compound as a liquid (145 mg, 46% yield, two steps).1H-NMR (600 MHz; DMSO-d6): δ 11.26 (brs, 1H), 7.31 (dd, 1H), 6.93 (d, 1H), and 6.90 (d, 1H), 6.29 (dd, 1H), 3.78 (s, 3H).

References

[1] Patent: WO2013/61305, 2013, A1. Location in patent: Page/Page column 45; 46

4-BROMO-6-METHOXYINDOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-BROMO-6-METHOXYINDOLE manufacturers

Career Henan Chemical Co

Product: 4-BROMO-6-METHOXYINDOLE 393553-55-4
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-12

393553-55-4, 4-BROMO-6-METHOXYINDOLERelated Search:

6-BROMO-4-METHOXYINDOLE 3-Bromo-5-methoxyindole 3-Bromo-5-methoxyindole, N-BOC protected 98%,3-BROMO-5-METHOXYINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER,3-BROMO-5-METHOXYINDOLE, N-BOC PROTECTED 7-BROMO-4-METHOXYINDOLE 4-BROMO-6,7-DIMETHOXY-1H-INDOLE-2-CARBOXYLIC ACID METHYL ESTER 4-BROMO-6,7-DIMETHOXY-1H-INDOLE-2-CARBOXYLIC ACID 5-Bromo-8H-1,3-dioxa-8-aza-as-indacene-7-carboxylic acid 4-BROMO-6-METHOXYINDOLE 4-BROMO-7-ETHOXY-6-METHOXY-1H-INDOLE-2-CARBOXYLIC ACID METHYL ESTER 5-BROMO-8H-1,3-DIOXA-8-AZA-AS-INDACENE-7-CARBOXYLIC ACID METHYL ESTER BROMOHARMALINE, HBR 4-BROMO-6-ETHOXY-7-METHOXY-1H-INDOLE-2-CARBOXYLIC ACID 4-BROMO-7-ETHOXY-6-METHOXY-1H-INDOLE-2-CARBOXYLIC ACID BROMOHARMINE HBR

4-BROMO-6-METHYLOXY INDOLE

4-bromo-6-methoxy-1H-indole

1H-Indole, 4-broMo-6-Methoxy-

4-broMo-6-Methyloxyl indole

4-BROMO-6-METHOXYINDOLE

393553-55-4