3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE
Uses- Product Name
- 3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE
- CAS No.
- 50608-99-6
- Chemical Name
- 3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE
- Synonyms
- 3-AMinopicolinaMide;H66691;3-Aminopyridin-2-carboxamide;3-aMino-2-PyridinecarboxaMide;3-AMINOPYRIDINE-2-CARBOXAMIDE;2-Pyridinecarboxamide, 3-amino-;2-Pyridinecarboxamide,3-amino-(9CI);3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE;3-Amino-pyridine-2-carboxylic acid amide 98%;3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE ISO 9001:2015 REACH
- CBNumber
- CB1393198
- Molecular Formula
- C6H7N3O
- Formula Weight
- 137.14
- MOL File
- 50608-99-6.mol
3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- Appearance
- Off-white to yellow Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A576858
- Product name
- 3-Aminopyridine-2-carboxamide
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 119116
- Product name
- 3-Aminopicolinamide
- Purity
- 95+%
- Packaging
- 1g
- Price
- $252
- Updated
- 2021/12/16
- Product number
- FA56520
- Product name
- 3-Aminopyridine-2-carboxylic acid amide
- Packaging
- 2g
- Price
- $260
- Updated
- 2021/12/16
- Product number
- FA56520
- Product name
- 3-Aminopyridine-2-carboxylic acid amide
- Packaging
- 100mg
- Price
- $40
- Updated
- 2021/12/16
- Product number
- FA56520
- Product name
- 3-Aminopyridine-2-carboxylic acid amide
- Packaging
- 500mg
- Price
- $100
- Updated
- 2021/12/16
3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE Chemical Properties,Usage,Production
Uses
3-Aminopyridine-2-carboxamide is an amide derivative that can be used as a pharmaceutical intermediate.
Synthesis
51674-77-2
50608-99-6
171347-62-9
General procedure for the synthesis of 4-anilino-pyrido[3,2-d]pyrimidine methanesulfonate from 4-chloropyrido[3,2-d]pyrimidine: 4-chloropyrido[3,2-d]pyrimidine (84 mg, 0.5 mmol), aniline (56 mg, 0.6 mmol), and triethylamine (62 mg, 0.6 mmol) were dissolved in ethanol (2 mL) under nitrogen protection. reflux stirring for 2 hours. Upon completion of the reaction, the crude product was purified by preparative thin layer chromatography plate (silica gel) using chloroform solution containing 3% methanol as eluent. The major bands were collected, concentrated to dryness under reduced pressure, and the residual solids were dissolved in acetone (5 mL), filtered, and methanesulfonic acid (32 μL, 0.5 mmol) was added slowly. The precipitate was collected by filtration, washed with acetone and dried in a vacuum oven to afford 4-anilino-pyrido[3,2-d]pyrimidine methanesulfonate (91 mg, 57% yield) as dark yellow needle-like crystals.1H NMR (DMSO) δ 11.75 (1H, s, br), 9.11 (1H, dd, J = 1.5, 4.3 Hz), 8.97 (1H, s ), 8.32 (1H, dd, J = 1.5, 8.4 Hz), 8.12 (1H, dd, J = 4.3, 8.5 Hz), 7.88 (2H, d, J = 8.2 Hz), 7.49 (2H, t, J = 8.0 Hz), 7.32 (1H, t, J = 7.0 Hz), 2.34 (3H, s).
References
[1] Patent: US5654307, 1997, A
3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE manufacturers
- Product
- 3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE 50608-99-6
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.0% min
- Supply Ability
- 100 tons min
- Release date
- 2021-04-30
- Product
- 3-AMINO-PYRIDINE-2-CARBOXYLIC ACID AMIDE 50608-99-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1ton
- Release date
- 2019-07-11