1-BROMO-5-METHYLHEXANE
- Product Name
- 1-BROMO-5-METHYLHEXANE
- CAS No.
- 35354-37-1
- Chemical Name
- 1-BROMO-5-METHYLHEXANE
- Synonyms
- TIMTEC-BB SBB008833;1-BROMO-5-METHYLHEXANE;Hexane, 1-bromo-5-methyl-
- CBNumber
- CB1409031
- Molecular Formula
- C7H15Br
- Formula Weight
- 179.1
- MOL File
- 35354-37-1.mol
1-BROMO-5-METHYLHEXANE Property
- Melting point:
- 162-163°C
- Boiling point:
- 162-163°C
- Density
- 1,103 g/cm3
- refractive index
- 1.4485
- Flash point:
- 57°C
- storage temp.
- 2-8°C
- solubility
- Acetonitrile (Slightly), Chloroform (Slightly)
- form
- Oil
- color
- Colourless
- Water Solubility
- Not miscible with water.
- BRN
- 1731802
- InChI
- InChI=1S/C7H15Br/c1-7(2)5-3-4-6-8/h7H,3-6H2,1-2H3
- InChIKey
- XAOFMTDKQYEOES-UHFFFAOYSA-N
- SMILES
- C(Br)CCCC(C)C
- CAS DataBase Reference
- 35354-37-1(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H226Flammable liquid and vapour
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 8044BA
- Product name
- 1-Bromo-5-methylhexane
- Packaging
- 250mg
- Price
- $95
- Updated
- 2021/12/16
- Product number
- 8044BA
- Product name
- 1-Bromo-5-methylhexane
- Packaging
- 5g
- Price
- $308
- Updated
- 2021/12/16
- Product number
- A544903
- Product name
- 1-Bromo-5-methylhexane
- Purity
- 95+%
- Packaging
- 100mg
- Price
- $18
- Updated
- 2021/12/16
- Product number
- A544903
- Product name
- 1-Bromo-5-methylhexane
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $18
- Updated
- 2021/12/16
- Product number
- A544903
- Product name
- 1-Bromo-5-methylhexane
- Purity
- 95+%
- Packaging
- 5g
- Price
- $63
- Updated
- 2021/12/16
1-BROMO-5-METHYLHEXANE Chemical Properties,Usage,Production
Uses
Isoheptyl Bromide is a useful chemical reagent.
Synthesis
951405-21-3
35354-37-1
Synthesis of 1-bromo-5-methylhexane (25): to a stirred solution of LiBr (6.26 g, 72.0 mmol) in DMF (40 mL) was slowly added a solution of compound 24 (6.60 g, 24.4 mmol) in DMF (6 mL). The reaction mixture was stirred continuously at 45 °C for 3 hours. Upon completion of the reaction, the reaction was quenched by the addition of water (100 mL) and the reaction product was extracted several times with ether (5 × 250 mL). The organic phases were combined and concentrated under reduced pressure to remove the solvent to give the crude product. After purification, the target product 25 (2.40 g, 13.4 mmol, 55% yield) was obtained. The structure of the product was determined by 1H NMR (400 MHz, CDCl3) δ 0.88 (6H, d, J = 6.6 Hz), 1.19 (2H, m), 1.42 (2H, m), 1.54 (1H, m), 1.83 (2H, m), 3.41 (2H, t, J = 6.9 Hz); 13C NMR (100 MHz, CDCl3) δ 22.5, 26.0, 27.8, 33.1, 34.1, 38.0; MS (EI) m/z 179 (M+, 80), 163 (14), 155 (9), 137 (100); exact mass calculated value C6H12Br ([M-CH3]+) 163.0122, confirmed by measured value 163.0121.
References
[1] Patent: US2007/238705, 2007, A1. Location in patent: Page/Page column 9; 13
[2] Patent: US2007/238701, 2007, A1. Location in patent: Page/Page column 12
[3] Patent: US2007/238702, 2007, A1. Location in patent: Page/Page column 11
[4] Patent: US2007/238706, 2007, A1. Location in patent: Page/Page column 9; 12
1-BROMO-5-METHYLHEXANE Preparation Products And Raw materials
Raw materials
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View Lastest Price from 1-BROMO-5-METHYLHEXANE manufacturers
- Product
- 1-BROMO-5-METHYLHEXANE 35354-37-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 85.0-99.8%
- Supply Ability
- 200kg
- Release date
- 2019-08-30