ETHYL 3-PYRIDYLACETATE
Uses- Product Name
- ETHYL 3-PYRIDYLACETATE
- CAS No.
- 39931-77-6
- Chemical Name
- ETHYL 3-PYRIDYLACETATE
- Synonyms
- ethyl 2-(pyridin-3-yl)acetate;LABOTEST-BB LT00847594;ETHYL 3-PYRIDYLACETATE;Ethyl 3-pyridineacetate;Ethyl 3-pyridinecacetate;ETHYL PYRIDINE-3-ACETATE;Ethyl 3-pyridinylacetate;Ethyl3-Pyridylacetate>Ethyl3-pyridylacetate,99%;Ethyl 3-pyridylacetate 99%
- CBNumber
- CB1426667
- Molecular Formula
- C9H11NO2
- Formula Weight
- 165.19
- MOL File
- 39931-77-6.mol
ETHYL 3-PYRIDYLACETATE Property
- Boiling point:
- 80 °C/0.4 mmHg (lit.)
- Density
- 1.086 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.500(lit.)
- Flash point:
- >230 °F
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- Chlorofrom (Slightly), Methanol (Slightly)
- pka
- 4.82±0.10(Predicted)
- form
- Liquid
- color
- Clear colorless to yellow
- BRN
- 123827
- InChIKey
- RPWXYCRIAGBAGY-UHFFFAOYSA-N
- CAS DataBase Reference
- 39931-77-6(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- E47255
- Product name
- Ethyl 3-pyridylacetate
- Purity
- 99%
- Packaging
- 5g
- Price
- $101
- Updated
- 2023/01/07
- Product number
- E47255
- Product name
- Ethyl 3-pyridylacetate
- Purity
- 99%
- Packaging
- 25g
- Price
- $271
- Updated
- 2023/01/07
- Product number
- E0874
- Product name
- Ethyl 3-Pyridylacetate
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $78
- Updated
- 2025/07/31
- Product number
- E925870
- Product name
- Ethyl 3-Pyridylacetate
- Packaging
- 10g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- J94443
- Product name
- Ethyl 3-Pyridylacetate
- Packaging
- 1g
- Price
- $10
- Updated
- 2021/12/16
ETHYL 3-PYRIDYLACETATE Chemical Properties,Usage,Production
Uses
Ethyl 3-Pyridylacetate is a reagent in the preparation of piperidinylalkanoic acid derivatives as a potent α4β1 integrin antagonists.
Chemical Properties
clear colorless to yellow liquid
Uses
Ethyl 3-Pyridylacetate is a reagent in the preparation of piperidinylalkanoic acid derivatives as a potent α4β1 integrin antagonists.
Synthesis
626-55-1
6148-64-7
39931-77-6
General procedure: After evacuation under a standard cycle and backfilling with dry pure nitrogen, palladium catalyst (see Tables 1, 2, 3, and 4 for amounts), ligand (see Tables 1, 2, 3, and 4), N,N-dimethylpyridin-4-amine (DMAP, see Tables 1, 2, 3, and 4), and monoethyl malonate potassium salt (see Tables 1, 2, 3, and 4) were added sequentially to the oven-dried Schlenk tubes fitted with a magnetic stir bar. and Table 4), and monoethyl malonate potassium salt (see Tables 1, 2, 3, and 4 for amounts). Subsequently, the Schlenk tubes were evacuated and backfilled with argon, and this process was repeated three times. Under argon protection, 3-bromopyridine (see Tables 1, 2, 3, and 4 for amounts) and solvent (see Tables 1, 2, 3, and 4 for types and amounts) were added via syringe. The Schlenk tube was sealed and stirred for 10 minutes at room temperature. After that, the Schlenk tube was connected to an argon-filled Schlenk line and placed in an oil bath preheated to 140-150°C and the reaction was stirred for 20-25 hours. After completion of the reaction, the reaction mixture was cooled to room temperature, diluted with ether and the yield of ethyl 3-pyridylacetate was determined by gas chromatography using 1,3-dimethoxybenzene as an internal standard.
References
[1] Tetrahedron, 2012, vol. 68, # 9, p. 2113 - 2120
ETHYL 3-PYRIDYLACETATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from ETHYL 3-PYRIDYLACETATE manufacturers
- Product
- ETHYL 3-PYRIDYLACETATE 39931-77-6
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-26
- Product
- ETHYL 3-PYRIDYLACETATE 39931-77-6
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 95%-99%
- Supply Ability
- 100KG
- Release date
- 2019-08-29