3-CYANO-5-NITROINDOLE
- Product Name
- 3-CYANO-5-NITROINDOLE
- CAS No.
- 7147-14-0
- Chemical Name
- 3-CYANO-5-NITROINDOLE
- Synonyms
- 3-CYANO-5-NITROINDOLE;5-Nitroindole-3-carbonitrile;1H-Indole-3-carbonitrile, 5-nitro-
- CBNumber
- CB1664719
- Molecular Formula
- C9H5N3O2
- Formula Weight
- 187.15
- MOL File
- 7147-14-0.mol
3-CYANO-5-NITROINDOLE Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Yellow to brown Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CHM0094344
- Product name
- 3-CYANO-5-NITROINDOLE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.98
- Updated
- 2021/12/16
- Product number
- 5482CB
- Product name
- 5-Nitro-1H-indole-3-carbonitrile
- Packaging
- 1g
- Price
- $532
- Updated
- 2021/12/16
- Product number
- CD11068253
- Product name
- 5-Nitro-1H-indole-3-carbonitrile
- Purity
- 97%
- Packaging
- 10g
- Price
- $539
- Updated
- 2021/12/16
- Product number
- SC-37332
- Product name
- 5-nitro-1H-indole-3-carbonitrile
- Purity
- 95
- Packaging
- 5g
- Price
- $2017
- Updated
- 2021/12/16
- Product number
- CM148751
- Product name
- 5-Nitro-1H-indole-3-carbonitrile
- Purity
- 95%+
- Packaging
- 10g
- Price
- $509
- Updated
- 2021/12/16
3-CYANO-5-NITROINDOLE Chemical Properties,Usage,Production
Uses
3-Cyano-5-nitroindole is mainly used in pharmaceutical synthesis and organic experiments.
Synthesis
6146-52-7
140-29-4
7147-14-0
GENERAL METHOD: A mixture of CuI (0.6 mmol), 5-nitroindole (0.5 mmol), and phenylacetonitrile (0.6 mmol) in DMF (3.0 mL) was placed in air and reacted with stirring for 34 h at 100 °C, followed by cooling to room temperature. Upon completion of the reaction, the reaction mixture was quenched with 10 mL of water followed by extraction with dichloromethane (DCM, 3 x 10 mL). The organic layers were combined, washed with saturated aqueous sodium chloride solution and dried with anhydrous magnesium sulfate (MgSO?). Finally, the solution was concentrated under reduced pressure and purified by column chromatography to afford the target product 5-nitroindole-3-carbonitrile.
References
[1] Tetrahedron, 2013, vol. 69, # 21, p. 4236 - 4240
3-CYANO-5-NITROINDOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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