ChemicalBook > CAS DataBase List > 1,4-Cyclohexanedione bis(ethylene ketal)

1,4-Cyclohexanedione bis(ethylene ketal)

Product Name: 1,4-Cyclohexanedione bis(ethylene ketal)
CAS No.: 183-97-1
Chemical Name: 1,4-Cyclohexanedione bis(ethylene ketal)
Synonyms: 1,4-Cyclohexanedione diethylene ketal;1,4-CYCLOHEXANEDIONE BIS(ETHYLENEKETAL);1,4-CYCLOHEXANEDIONE BISETHYLENE KETAL F;1,4-CYCLOHEXANEDIONE BIS(ETHYLENE ACETAL);1,4-Cyclohexianedione bis(ethylene acetal);1,4-Cyclohexanedione Bis(ethyleneketal) >1,4,9,12-TETRAOXADISPIRO[4.2.4.2]TETRADECANE;2,5-bis(butylamino)cyclohexa-2,5-diene-1,4-dione;1,4-Cyclohexanedione bis(ethylene glycol) diketal;1,4,9,12-tetraoxadispiro[4.2.4^{8}.2^{5}]tetradecane
CBNumber: CB1668030
Molecular Formula: C10H16O4
Formula Weight: 200.23
MOL File: 183-97-1.mol

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1,4-Cyclohexanedione bis(ethylene ketal) Property

Melting point:: 79-80 °C (lit.)
Boiling point:: 75-85 °C/0.5 mmHg (lit.)
Density: 1.1508 (rough estimate)
refractive index: 1.4459 (estimate)
Flash point:: 75-85°C/0.5mm
storage temp.: Store below +30°C.
form: powder to crystal
color: White to Almost white
InChI: InChI=1S/C10H16O4/c1-2-10(13-7-8-14-10)4-3-9(1)11-5-6-12-9/h1-8H2
InChIKey: YSMVSEYPOBXSOK-UHFFFAOYSA-N
SMILES: O1C2(CCC3(OCCO3)CC2)OCC1
CAS DataBase Reference: 183-97-1(CAS DataBase Reference)
NIST Chemistry Reference: 1,4-Cyclohexanedione bis(ethylene ketal)(183-97-1)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-37/39
WGK Germany: 3
HS Code: 29329990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 298743
Product name: 1,4-Cyclohexanedione bis(ethylene ketal)
Purity: 99%
Packaging: 10g
Price: $96.8
Updated: 2023/06/20

TCI Chemical

Product number: C1544
Product name: 1,4-Cyclohexanedione Bis(ethyleneketal)
Purity: >99.0%(GC)
Packaging: 25g
Price: $186
Updated: 2025/07/31

TRC

Product number: C992225
Product name: 1,4-Cyclohexanedione bis(ethylene ketal)
Packaging: 500mg
Price: $60
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0006106
Product name: 1,4-CYCLOHEXANEDIONE BIS(ETHYLENE ACETAL)
Purity: 95.00%
Packaging: 25G
Price: $1200.75
Updated: 2021/12/16

Ambeed

Product number: A450819
Product name: 1,4,9,12-Tetraoxadispiro[4.2.4.2]tetradecane
Purity: 98%
Packaging: 5g
Price: $25
Updated: 2021/12/16

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1,4-Cyclohexanedione bis(ethylene ketal) Chemical Properties,Usage,Production

General Description

Hydrolysis of 1,4-cyclohexanedione bis(ethylene ketal) at 250°C has been reported.

Synthesis

After mixing 2243 g (20 mol) of 1,4-cyclohexanedione, 2607 g (42 mol) of ethylene glycol, the resin filtered, and 26 L of toluene, the temperature was raised slowly and refluxed for 11 hours to separate the water. The reaction temperature was lowered to 40° C., the resin was filtered, and the organic phase was concentrated until no liquid flowed. Then add 1257g (21mol) of methylboronic acid and 20L of n-heptane, raise the temperature to 80°C and react for 6 hours, then slowly cool down to 5-10°C in a gradient, filter, rinse the filter cake with n-heptane, and dry to obtain 1,4-Cyclohexanedione bis(ethylene ketal).

1,4-Cyclohexanedione bis(ethylene ketal) Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,4-Cyclohexanedione bis(ethylene ketal) manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 1,4-Cyclohexanedione bis(ethylene ketal) 183-97-1
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99.0%
Supply Ability: 1000KG
Release date: 2024-07-24

Career Henan Chemical Co

Product: 1,4-Cyclohexanedione bis(ethylene ketal) 183-97-1
Price: US $5.50/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 1kg-100kg
Release date: 2020-01-14

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183-97-1

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