ChemicalBook > CAS DataBase List > TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE

TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE

Product Name: TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE
CAS No.: 183741-80-2
Chemical Name: TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE
Synonyms: 3-(Boc-amino)-6-methoxypyridine;tert-Butyl (6-methoxypyridin-3-yl);tert-butyl 6-Methoxypyridin-3-ylcarbaMate;TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE;tert-Butyl N-(6-methoxypyridin-3-yl)carbamate;(6-Methoxy-pyridin-3-yl)-carbaMic acid tert-butyl ester;(6-Methoxy-3-pyridinyl)-carbamic acid 1,1-dimethylethyl ester;Carbamic acid, N-(6-methoxy-3-pyridinyl)-, 1,1-dimethylethyl ester
CBNumber: CB1690048
Molecular Formula: C11H16N2O3
Formula Weight: 224.26
MOL File: 183741-80-2.mol

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TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE Property

Boiling point:: 278.6℃
Density: 1.146
Flash point:: 122.3℃
storage temp.: 2-8°C
pka: 12.34±0.70(Predicted)
Appearance: Off-white to pale purple Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: T135780
Product name: tert-Butyl6-Methoxypyridin3-ylcarbamate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB54415
Product name: tert-Butyl-n-(6-methoxy-3-pyridyl)carbamate
Packaging: 250mg
Price: $77.5
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB54415
Product name: tert-Butyl-n-(6-methoxy-3-pyridyl)carbamate
Packaging: 500mg
Price: $125
Updated: 2021/12/16

AK Scientific

Product number: Z3431
Product name: tert-ButylN-(6-methoxypyridin-3-yl)carbamate
Packaging: 1g
Price: $278
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB54415
Product name: tert-Butyl-n-(6-methoxy-3-pyridyl)carbamate
Packaging: 1g
Price: $316.3
Updated: 2021/12/16

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TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE Chemical Properties,Usage,Production

Synthesis

6628-77-9

24424-99-5

183741-80-2

The general procedure for the synthesis of 3-(Boc-amino)-6-methoxypyridine from 5-amino-2-methoxypyridine and di-tert-butyl dicarbonate was as follows: 1.0 g of 5-amino-2-methoxypyridine was placed in a single-neck flask and dissolved in 40 mL of dioxane. Subsequently 1.79 g of di-tert-butyl dicarbonate was added and the reaction mixture was heated to reflux overnight. After completion of the reaction, it was cooled to room temperature and the solvent was removed by evaporation under reduced pressure. The resulting residue was purified by silica gel column chromatography using a solvent mixture of heptane and ethyl acetate (the volume ratio was tapered from 90/10 to 70/30) as eluent for gradient elution. Finally, 1.58 g of the target product 3-(Boc-amino)-6-methoxypyridine was obtained in 97% yield.

References

[1] Patent: US2011/178053, 2011, A1. Location in patent: Page/Page column 46
[2] Bioorganic and Medicinal Chemistry Letters, 2004, vol. 14, # 12, p. 3303 - 3306
[3] Journal of the Chemical Society - Perkin Transactions 1, 1996, # 18, p. 2221 - 2226
[4] Tetrahedron Letters, 2011, vol. 52, # 41, p. 5292 - 5296
[5] Journal of Medicinal Chemistry, 2015, vol. 58, # 12, p. 5053 - 5074

TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE Preparation Products And Raw materials

Raw materials

Preparation Products

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TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE Suppliers

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View Lastest Price from TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE manufacturers

Shanghai Rlavie Technology Co ltd

Product: tert-Butyl-n-(6-Methoxy-3-pyridyl)carbaMate 183741-80-2
Price: US $0.00-0.00/g
Min. Order: 1g
Purity: 98%minNMR
Supply Ability: 50kgs/month
Release date: 2022-04-17

183741-80-2, TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATERelated Search:

5-(TERT-BUTOXYCARBONYLAMINO)-2-METHOXYPYRIDINE-4-CARBOXYLIC ACID 3-(BOC-AMINO)PYRIDINE 3-TERT-BUTYLOXYCARBONYLAMINO-6-METHOXYPYRIDINE-2-BORONIC ACID PINACOL ESTER 5-TERT-BUTYLOXYCARBONYLAMINO-2-METHOXYPYRIDINE-3-BORONIC ACID PINACOL ESTER TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE

TERT-BUTYL-N-(6-METHOXY-3-PYRIDYL)CARBAMATE

tert-Butyl N-(6-methoxypyridin-3-yl)carbamate

(6-Methoxy-pyridin-3-yl)-carbaMic acid tert-butyl ester

tert-butyl 6-Methoxypyridin-3-ylcarbaMate

3-(Boc-amino)-6-methoxypyridine

(6-Methoxy-3-pyridinyl)-carbamic acid 1,1-dimethylethyl ester

tert-Butyl (6-methoxypyridin-3-yl)

Carbamic acid, N-(6-methoxy-3-pyridinyl)-, 1,1-dimethylethyl ester

183741-80-2