(6-Chloro-2-pyridinyl)methanol
- Product Name
- (6-Chloro-2-pyridinyl)methanol
- CAS No.
- 33674-97-4
- Chemical Name
- (6-Chloro-2-pyridinyl)methanol
- Synonyms
- CHEMPACIFIC 38159;2-CHLORO-6-PICOLYL ALCOHOL;2-Chloropyridine-6-Methanol;6-Chloro-2-pyridinemethanol;2-Pyridinemethanol, 6-chloro-;(6-Chloro-2-pyridinyl)methanol;(6-CHLORO-PYRIDIN-2-YL)-METHANOL;2-Hydroxymethyl-6-chloro-pyridine;2-Chloro-6-(Hydroxymethyl)Pyridine;(6-Chloro-2-pyridinyl)methanol ISO 9001:2015 REACH
- CBNumber
- CB1693089
- Molecular Formula
- C6H6ClNO
- Formula Weight
- 143.57
- MOL File
- 33674-97-4.mol
(6-Chloro-2-pyridinyl)methanol Property
- Boiling point:
- 251.8±25.0 °C(Predicted)
- Density
- 1.324±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 13.12±0.10(Predicted)
- form
- liquid
- color
- Colourless
Safety
- HazardClass
- IRRITANT
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B419250
- Product name
- (6-Chloro-2-pyridinyl)methanol
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 046755
- Product name
- (6-Chloro-2-pyridinyl)methanol
- Purity
- 95+%
- Packaging
- 5g
- Price
- $88
- Updated
- 2021/12/16
- Product number
- OR303659
- Product name
- (6-Chloro-2-pyridinyl)methanol
- Packaging
- 1g
- Price
- $21
- Updated
- 2021/12/16
- Product number
- 046755
- Product name
- (6-Chloro-2-pyridinyl)methanol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $28
- Updated
- 2021/12/16
- Product number
- 4H56-5-H4
- Product name
- (6-Chloro-2-pyridinyl)methanol
- Packaging
- 1g
- Price
- $37
- Updated
- 2021/12/16
(6-Chloro-2-pyridinyl)methanol Chemical Properties,Usage,Production
Synthesis
6636-55-1
33674-97-4
General procedure for the synthesis of 2-chloro-6-hydroxymethylpyridine from methyl 6-chloropyridine-2-carboxylate: 6.7 g (39.0 mmol) of methyl 6-chloropyridine-2-carboxylate was dissolved in 90 mL of anhydrous tetrahydrofuran, which was subsequently cooled to -45 °C. A 40 mL solution of 1 M lithium aluminum hydride in tetrahydrofuran was added slowly and dropwise over 30 min. The reaction mixture was stirred at -45°C for 30 minutes and then slowly warmed to 0°C and continued stirring for 30 minutes. Subsequently, 15 mL of 1 N aqueous sodium hydroxide solution was slowly added dropwise to quench the reaction. Solid impurities were removed by diatomaceous earth filtration and the filtrate was concentrated to give 5.08 g (35.4 mmol, 91% yield) of 2-chloro-6-hydroxymethylpyridine. The product was characterized by 1H NMR (CDCl3, ppm): δ 7.61 (1H, d), 7.30 (1H, t), 7.04 (1H, d), 3.72 (2H, s).FAB MS (m/z) = 144 [M + 1].
References
[1] Patent: WO2007/58482, 2007, A1. Location in patent: Page/Page column 47-48
(6-Chloro-2-pyridinyl)methanol Preparation Products And Raw materials
Raw materials
Preparation Products
(6-Chloro-2-pyridinyl)methanol Suppliers
- Tel
- 17502177640
- 977963479@qq.com
- Country
- China
- ProdList
- 19
- Advantage
- 58
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9310
- Advantage
- 66
- Tel
- 021-50795510 4000665055
- Fax
- 021-50795055
- sales@accelachem.com
- Country
- China
- ProdList
- 11035
- Advantage
- 64
- Tel
- 021-58099652-8005 13585536065
- Fax
- 021-58099609
- bin.wu@shlschem.com
- Country
- China
- ProdList
- 9883
- Advantage
- 59
- Tel
- 86-0571-85151182
- Fax
- 86-0571-85151182
- Country
- China
- ProdList
- 5691
- Advantage
- 66
- Tel
- 13761627472
- Fax
- 86-21-64965863
- 183009664@qq.com
- Country
- China
- ProdList
- 649
- Advantage
- 62
- Tel
- 0086-21-58956006
- Fax
- 0086-21-58956100
- Country
- China
- ProdList
- 7811
- Advantage
- 57
View Lastest Price from (6-Chloro-2-pyridinyl)methanol manufacturers
- Product
- (6-Chloro-2-pyridinyl)methanol 33674-97-4
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-08-27
- Product
- (6-Chloro-2-pyridinyl)methanol 33674-97-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-31