2-Amino-4-methylbenzamide

Product Name: 2-Amino-4-methylbenzamide
CAS No.: 39549-79-6
Chemical Name: 2-Amino-4-methylbenzamide
Synonyms: -Amino-4-methylbenzamide;2-AMINO-4-METHYLBENZAMIDE;Benzamide, 2-amino-4-methyl-;2-Amino-4-methylbenzamide ,98%;Benzamide, 2-amino-4-methyl- (9CI)
CBNumber: CB1748932
Molecular Formula: C8H10N2O
Formula Weight: 150.18
MOL File: 39549-79-6.mol

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2-Amino-4-methylbenzamide Property

Melting point:: 147 °C
Boiling point:: 282.8±28.0 °C(Predicted)
Density: 1.185±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 15.98±0.50(Predicted)
Appearance: Light yellow to yellow Solid
CAS DataBase Reference: 39549-79-6(CAS DataBase Reference)

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Safety

Hazard Codes: Xn
Risk Statements: 36/37/38-20/21/22-36-22
Safety Statements: 26-36/37/39-36/37-36
HS Code: 29242100

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H317May cause an allergic skin reaction

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: A614633
Product name: 2-Amino-4-methylbenzamide
Packaging: 2.5g
Price: $330
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA139727
Product name: 2-Amino-4-methylbenzamide
Packaging: 10g
Price: $437.5
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4748-1-39
Product name: 2-amino-4-methylbenzamide
Packaging: 1g
Price: $152
Updated: 2021/12/16

Matrix Scientific

Product number: 081100
Product name: 2-Amino-4-methylbenzamide
Purity: 97%
Packaging: 1g
Price: $185
Updated: 2021/12/16

AK Scientific

Product number: W5989
Product name: 2-Amino-4-methylbenzamide
Packaging: 5g
Price: $201
Updated: 2021/12/16

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2-Amino-4-methylbenzamide Chemical Properties,Usage,Production

Synthesis

26830-96-6

39549-79-6

The general procedure for the synthesis of 2-amino-4-methylbenzamide using 2-amino-4-methylbenzonitrile as starting material was as follows: to a suspension of 2-amino-4-methylbenzonitrile (800 mg, 6.1 mmol) in water (1 mL), concentrated sulfuric acid (3 mL) was slowly added. The mixed solution was placed in an oil bath preheated to 120 °C and the reaction was stirred for 20 min. Immediately after completion of the reaction, the reaction mixture was cooled in an ice bath. Subsequently, the reaction solution was adjusted to alkaline by dropwise addition of 5% sodium hydroxide solution and the precipitated solid was collected by vacuum filtration. Finally, 484.4 mg of 2-amino-4-methylbenzamide was obtained in 53% yield as a light brown solid. The product was characterized by 1H NMR (DMSO-d6): δ 7.63 (br s, 1H), 7.42 (d, 1H), 6.95 (br s, 1H), 6.55 (br s, 2H), 6.45-6.48 (m, 1H), 6.29 (ddd, 1H), 2.16 (s, 3H). The mass spectrum (ES) showed a m/z of 134 (M-16).

References

[1] Journal of the American Chemical Society, 2008, vol. 130, # 47, p. 15786 - 15787
[2] Journal of Organic Chemistry, 2006, vol. 71, # 1, p. 382 - 385
[3] Patent: WO2006/74223, 2006, A2. Location in patent: Page/Page column 51
[4] Patent: WO2013/100632, 2013, A1. Location in patent: Page/Page column 49; 50
[5] Patent: US2014/371219, 2014, A1. Location in patent: Paragraph 0342; 0343

2-Amino-4-methylbenzamide Preparation Products And Raw materials

Raw materials

Ethanol Hydrochloric acid Sodium hydroxide 2-Amino-4-methylbenzoic acid Thionyl chloride Ammonia

Preparation Products

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2-Amino-4-methylbenzamide Suppliers

Belgium 1 China 71 Europe 1 France 1 Germany 2 India 1 The Netherlands 1 United Kingdom 10 United States 16 Global 104

J & K SCIENTIFIC LTD.

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Shanghai Raise Chemical Technology Co.,Ltd

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View Lastest Price from 2-Amino-4-methylbenzamide manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 2-Amino-4-methylbenzamide 39549-79-6
Price: US $2.20-8.80/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2025-06-17

Career Henan Chemical Co

Product: 2-Amino-4-methylbenzamide 39549-79-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 98% HPLC
Supply Ability: 10 tons
Release date: 2020-02-14

39549-79-6, 2-Amino-4-methylbenzamideRelated Search:

Disperse Blue 60 2-Amino-4-methylbenzamide 4,11-diamino-1H-naphth[2,3-f]isoindole-1,3,5,10(2H)-tetrone ACTINOMYCIN V Actinomycin D 7-AMINOACTINOMYCIN D 8-CARBOXYLIC-3H-1,4-BENZODIAZEPIN-2,5-(1H,4H)-DIONE 2-AMINO-N-METHYLBENZAMIDE 3-AMINOBENZOYLMETHYLAMIDE 4-Amino-N-methylbenzamide 2-AMINO-5-METHYLBENZAMIDE 3-Amino-4-methylbenzamide BENZAMIDINE 2-[(diphenylacetyl)amino]-N-methylbenzamide 2-[(cyclopropylcarbonyl)amino]-N-methylbenzamide ACTINOMYCIN I FROM STREPTOMYCESANTIBIOTI CUS BUTTPARK 19\04-18 BUTTPARK 19\04-13

2-AMINO-4-METHYLBENZAMIDE

Benzamide, 2-amino-4-methyl- (9CI)

2-Amino-4-methylbenzamide ,98%

-Amino-4-methylbenzamide

Benzamide, 2-amino-4-methyl-

39549-79-6

AMIDE

Amines

Phenyls & Phenyl-Het