ChemicalBook > CAS DataBase List > 4-NITROPHENYL-2-METHOXYETHYL ETHER

4-NITROPHENYL-2-METHOXYETHYL ETHER

Product Name
4-NITROPHENYL-2-METHOXYETHYL ETHER
CAS No.
22483-40-5
Chemical Name
4-NITROPHENYL-2-METHOXYETHYL ETHER
Synonyms
SKL382;1-(2-Methoxyethoxy);4-NITROPHENYL-2-METHOXYETHYL ETHER;Benzene, 1-(2-methoxyethoxy)-4-nitro-
CBNumber
CB1789113
Molecular Formula
C9H11NO4
Formula Weight
197.19
MOL File
22483-40-5.mol
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4-NITROPHENYL-2-METHOXYETHYL ETHER Property

Melting point:
87 °C
Boiling point:
317.0±22.0 °C(Predicted)
Density 
1?+-.0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
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Safety

HS Code 
2909309090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P273Avoid release to the environment.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M304498
Product name
1-(2-Methoxyethoxy)-4-nitrobenzene
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
M304498
Product name
1-(2-Methoxyethoxy)-4-nitrobenzene
Packaging
500mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
J96335
Product name
1-(2-Methoxyethoxy)-4-nitrobenzene
Packaging
1g
Price
$22
Updated
2021/12/16
AK Scientific
Product number
Z4445
Product name
1-(2-Methoxyethoxy)-4-nitrobenzene
Packaging
1g
Price
$29
Updated
2021/12/16
Matrix Scientific
Product number
119927
Product name
1-(2-Methoxyethoxy)-4-nitrobenzene
Purity
95+%
Packaging
1g
Price
$78
Updated
2021/12/16
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4-NITROPHENYL-2-METHOXYETHYL ETHER Chemical Properties,Usage,Production

Synthesis

100-02-7

6482-24-2

22483-40-5

To a solution of N,N-dimethylformamide (DMF, 10 mL) of 4-nitrophenol (2.78 g, 20 mmol) and 2-bromoethyl methyl ether (3.6 g, 26 mmol) was added anhydrous potassium carbonate (K2CO3, 5.52 g, 40 mmol). The reaction mixture was stirred at 80 °C for 5 hours. Upon completion of the reaction, the mixture was cooled to room temperature and the reaction was subsequently quenched with deionized water (30 mL) and ethyl acetate (EtOAc, 40 mL). The organic and aqueous layers were separated and the aqueous layer was further extracted with ethyl acetate (2 x 25 mL). All organic extracts were combined, washed with saturated sodium chloride solution (brine, 2×20 mL), dried over anhydrous sodium sulfate (Na2SO4), and concentrated under reduced pressure to afford the target product, 4-nitrophenyl-2-methoxyethyl ether (3.9 g, 100% yield) as a yellow solid.

References

[1] Patent: WO2014/130693, 2014, A1. Location in patent: Paragraph 00544; 00546
[2] Patent: WO2015/6754, 2015, A2. Location in patent: Paragraph 00243; 00244
[3] European Journal of Medicinal Chemistry, 1980, vol. 15, # 5, p. 399 - 404
[4] Patent: US2005/277668, 2005, A1. Location in patent: Page/Page column 17

4-NITROPHENYL-2-METHOXYETHYL ETHER Preparation Products And Raw materials

Raw materials

Preparation Products

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22483-40-5, 4-NITROPHENYL-2-METHOXYETHYL ETHERRelated Search:

4-NITROBENZO-18-CROWN-6 4-NITROPHENYL-2-METHOXYETHYL ETHER 1,2-EPOXY-3-(4-NITROPHENOXY)PROPANE 4-NITROBENZO-15-CROWN-5 Diglyme BIS(2,4-DINITROPHENYL) OXALATE 4'-NITRO-5'-(PICRYLAMINO)BENZO-18-CROWN-6 METHYL-((4-NITROPHENYL)-2,3,4-TRI-O-ACETYL-BETA-D-GLUCOPYRANOSIDE)URONATE 2-DODECYL-2-METHYL-1,3-PROPANEDIYL BIS[N-[5'-NITRO(BENZO-15-CROWN-5)-4'-YL]CARBAMATE] 2-[(3-methyl-4-nitrophenoxy)methyl]oxirane 4-NITRODIBENZO-18-CROWN-6, 97 1-(4-NITROPHENYL)-2,3,4,6-TETRA-O-ACETYL-BETA-D-GALACTOPYRANOSIDE (4-NITRO)PHENYL-2,3,4,6-TETRA-O-ACETYL-ALPHA-D-GALACTOPYRANOSIDE 2-(4-NITROPHENOXY) ETHYL METHACRYLATE (4-NITROPHENOXY) ACETIC ACID ETHYL ESTER 4'-AMINO-5'-NITROBENZO-15-CROWN-5 4-NITROPHENYL 3-BROMO-2,2-DIETHOXYPROPIONATE 1-[2-(2,4-DINITROPHENOXY)ETHOXY]-2,4-DINITROBENZENE

  • 4-NITROPHENYL-2-METHOXYETHYL ETHER
  • 1-(2-Methoxyethoxy)
  • Benzene, 1-(2-methoxyethoxy)-4-nitro-
  • SKL382
  • 22483-40-5