ChemicalBook > CAS DataBase List > 1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID

1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID

Product Name
1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID
CAS No.
23348-99-4
Chemical Name
1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID
Synonyms
1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID;Cyclopropanecarboxylic acid, 1-(4-nitrophenyl)-;1-(4-nitrophenyl)-1-cyclopropanecarboxylic acid;1-(4-nitrophenyl)cyclopropane-1-carboxylic acid
CBNumber
CB1798508
Molecular Formula
C10H9NO4
Formula Weight
207.18
MOL File
23348-99-4.mol
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1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID Property

Melting point:
190.5-193 °C
Boiling point:
403.8±38.0 °C(Predicted)
Density 
1.480±0.06 g/cm3(Predicted)
storage temp. 
Store at room temperature
pka
3.78±0.20(Predicted)
Appearance
Light yellow to khaki Solid
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Safety

HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
N926495
Product name
1-(4-Nitrophenyl)cyclopropanecarboxylicAcid
Packaging
10mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
1542AB
Product name
1-(4-Nitrophenyl)cyclopropanecarboxylicacid
Packaging
500mg
Price
$320
Updated
2021/12/16
Matrix Scientific
Product number
082896
Product name
1-(4-Nitrophenyl)cyclopropanecarboxylic acid
Purity
97%
Packaging
1g
Price
$488
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-1-8J
Product name
1-(4-Nitrophenyl)cyclopropanecarboxylic acid
Packaging
1g
Price
$784
Updated
2021/12/16
Crysdot
Product number
CD12093448
Product name
1-(4-Nitrophenyl)cyclopropanecarboxylicacid
Purity
95+%
Packaging
250mg
Price
$79
Updated
2021/12/16
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1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID Chemical Properties,Usage,Production

Synthesis

408328-42-7

23348-99-4

The general procedure for the synthesis of 1-(4-nitrophenyl)-cyclopropanecarboxylic acid was as follows: 1-(4-nitrophenyl)cyclopropanecarbonitrile (12.77 g, 67.16 mmol) was placed in a 250 mL three-necked round-bottomed flask and water (79 mL) and concentrated sulfuric acid (56 mL) were added. The reaction mixture was heated to reflux overnight and the reaction progress was monitored by thin layer chromatography (TLC) (Spreading agent: 100% ethyl acetate, product Rf value 0.49). After completion of the reaction, the reaction mixture was cooled and the precipitate was collected by filtration. The resulting solid was washed with distilled water (30 mL) and subsequently dried under vacuum overnight to afford the target product 1-(4-nitrophenyl)-cyclopropanecarboxylic acid (8.67 g, 41.45 mmol, 62% yield). The structure of the product was confirmed by 1H-NMR (DMSO-d6): δ 8.21-8.11 (d, 2H), 7.58-7.64 (d, 2H), 1.5-1.6 (t, 2H), 1.2-1.3 (t, 2H).

References

[1] Patent: WO2005/34837, 2005, A2. Location in patent: Page/Page column 46
[2] Patent: WO2005/34837, 2005, A2. Location in patent: Page/Page column 46
[3] Advanced Synthesis and Catalysis, 2018, vol. 360, # 22, p. 4306 - 4311

1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACID Suppliers

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23348-99-4, 1-(4-NITRO-PHENYL)-CYCLOPROPANECARBOXYLIC ACIDRelated Search:

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