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1-PHENYL-1H-INDOLE

Product Name
1-PHENYL-1H-INDOLE
CAS No.
16096-33-6
Chemical Name
1-PHENYL-1H-INDOLE
Synonyms
1-Phenylindole;1-PHENYL-1H-INDOLE;1-Pheny-1H-lindole;1H-Indole, 1-phenyl-
CBNumber
CB1819292
Molecular Formula
C14H11N
Formula Weight
193.24
MOL File
16096-33-6.mol
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1-PHENYL-1H-INDOLE Property

Melting point:
60-62℃
Boiling point:
190°C/20mmHg(lit.)
Density 
1.05±0.1 g/cm3 (20 ºC 760 Torr)
refractive index 
1.6580 to 1.6620
storage temp. 
Store at room temperature
form 
clear liquid
color 
Colorless to Yellow to Orange
InChI
InChI=1S/C14H11N/c1-2-7-13(8-3-1)15-11-10-12-6-4-5-9-14(12)15/h1-11H
InChIKey
YBFCBQMICVOSRW-UHFFFAOYSA-N
SMILES
N1(C2=CC=CC=C2)C2=C(C=CC=C2)C=C1
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Safety

HS Code 
2933.99.8290
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TCI Chemical
Product number
P2503
Product name
1-Phenyl-1H-indole
Purity
>98.0%(N)
Packaging
1g
Price
$69
Updated
2025/07/31
Chem-Impex
Product number
43004
Product name
1-Phenyl-1H-indole,≥97%(GC)
Purity
≥97%(GC)
Packaging
1G
Price
$75.11
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0093702
Product name
1-PHENYL-1H-INDOLE
Purity
95.00%
Packaging
5G
Price
$909.56
Updated
2021/12/16
AK Scientific
Product number
Z4239
Product name
1-Phenyl-1H-indole
Packaging
1g
Price
$1629
Updated
2021/12/16
Ambeed
Product number
A123443
Product name
1-Phenyl-1H-indole
Purity
98%
Packaging
100mg
Price
$14
Updated
2021/12/16
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1-PHENYL-1H-INDOLE Chemical Properties,Usage,Production

Synthesis

120-72-9

108-86-1

16096-33-6

1. indole (11.7 g, 0.1 mol) and bromobenzene (117 mL) were added to a four-necked flask, stirred and heated to 150-160°C for reflux. 2. cuprous chloride (2.47 g, 0.025 mol), L-proline (5.75 g, 0.05 mol) and potassium hydroxide (11.22 g, 0.2 mol) were added sequentially and the reaction was carried out for 8-12 h. The progress of the reaction was monitored by TLC. 3. After completion of the reaction, it was slightly cooled, the reaction mixture was filtered, the brown solid was washed with water, and the insoluble material cuprous chloride was dried and recycled. 4. The organic layer of the filtrate is washed with water and the bromobenzene is subsequently recovered by vacuum distillation. 5. 5. Finally, 1-phenylindole (17.76 g, 92.02% yield) was purified by distillation under reduced pressure.

References

[1] Journal of Organic Chemistry, 2001, vol. 66, # 23, p. 7729 - 7737
[2] Tetrahedron Letters, 2000, vol. 41, # 4, p. 481 - 483
[3] Tetrahedron Letters, 2017, vol. 58, # 32, p. 3155 - 3159
[4] New Journal of Chemistry, 2018, vol. 42, # 4, p. 2782 - 2789
[5] Comptes Rendus Chimie, 2018, vol. 21, # 7, p. 659 - 668

1-PHENYL-1H-INDOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-PHENYL-1H-INDOLE Suppliers

NovoChemy Ltd.
Tel
021-31261262/ 49 (0)17662837245
Fax
(0)21-33250524
Email
sales@novochemy.com
Country
Germany
ProdList
6328
Advantage
58
SYNTHON Chemicals GmbH & Co. KG
Tel
--
Fax
--
Email
synthon@synthon-chemicals.com
Country
Germany
ProdList
2000
Advantage
65
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View Lastest Price from 1-PHENYL-1H-INDOLE manufacturers

R&D Scientific Inc.
Product
1-Phenylindole 16096-33-6
Price
US $2600.00/g
Min. Order
1g
Purity
99
Supply Ability
500 Kg
Release date
2024-11-18
Career Henan Chemical Co
Product
1-PHENYL-1H-INDOLE 16096-33-6
Price
US $8.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
10tons
Release date
2018-12-24