1-PHENYL-1H-INDOLE
- Product Name
- 1-PHENYL-1H-INDOLE
- CAS No.
- 16096-33-6
- Chemical Name
- 1-PHENYL-1H-INDOLE
- Synonyms
- 1-Phenylindole;1-PHENYL-1H-INDOLE;1-Pheny-1H-lindole;1H-Indole, 1-phenyl-
- CBNumber
- CB1819292
- Molecular Formula
- C14H11N
- Formula Weight
- 193.24
- MOL File
- 16096-33-6.mol
1-PHENYL-1H-INDOLE Property
- Melting point:
- 60-62℃
- Boiling point:
- 190°C/20mmHg(lit.)
- Density
- 1.05±0.1 g/cm3 (20 ºC 760 Torr)
- refractive index
- 1.6580 to 1.6620
- storage temp.
- Store at room temperature
- form
- clear liquid
- color
- Colorless to Yellow to Orange
- InChI
- InChI=1S/C14H11N/c1-2-7-13(8-3-1)15-11-10-12-6-4-5-9-14(12)15/h1-11H
- InChIKey
- YBFCBQMICVOSRW-UHFFFAOYSA-N
- SMILES
- N1(C2=CC=CC=C2)C2=C(C=CC=C2)C=C1
Safety
- HS Code
- 2933.99.8290
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- P2503
- Product name
- 1-Phenyl-1H-indole
- Purity
- >98.0%(N)
- Packaging
- 1g
- Price
- $69
- Updated
- 2025/07/31
- Product number
- 43004
- Product name
- 1-Phenyl-1H-indole,≥97%(GC)
- Purity
- ≥97%(GC)
- Packaging
- 1G
- Price
- $75.11
- Updated
- 2021/12/16
- Product number
- CHM0093702
- Product name
- 1-PHENYL-1H-INDOLE
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $909.56
- Updated
- 2021/12/16
- Product number
- Z4239
- Product name
- 1-Phenyl-1H-indole
- Packaging
- 1g
- Price
- $1629
- Updated
- 2021/12/16
- Product number
- A123443
- Product name
- 1-Phenyl-1H-indole
- Purity
- 98%
- Packaging
- 100mg
- Price
- $14
- Updated
- 2021/12/16
1-PHENYL-1H-INDOLE Chemical Properties,Usage,Production
Synthesis
120-72-9
108-86-1
16096-33-6
1. indole (11.7 g, 0.1 mol) and bromobenzene (117 mL) were added to a four-necked flask, stirred and heated to 150-160°C for reflux. 2. cuprous chloride (2.47 g, 0.025 mol), L-proline (5.75 g, 0.05 mol) and potassium hydroxide (11.22 g, 0.2 mol) were added sequentially and the reaction was carried out for 8-12 h. The progress of the reaction was monitored by TLC. 3. After completion of the reaction, it was slightly cooled, the reaction mixture was filtered, the brown solid was washed with water, and the insoluble material cuprous chloride was dried and recycled. 4. The organic layer of the filtrate is washed with water and the bromobenzene is subsequently recovered by vacuum distillation. 5. 5. Finally, 1-phenylindole (17.76 g, 92.02% yield) was purified by distillation under reduced pressure.
References
[1] Journal of Organic Chemistry, 2001, vol. 66, # 23, p. 7729 - 7737
[2] Tetrahedron Letters, 2000, vol. 41, # 4, p. 481 - 483
[3] Tetrahedron Letters, 2017, vol. 58, # 32, p. 3155 - 3159
[4] New Journal of Chemistry, 2018, vol. 42, # 4, p. 2782 - 2789
[5] Comptes Rendus Chimie, 2018, vol. 21, # 7, p. 659 - 668
1-PHENYL-1H-INDOLE Preparation Products And Raw materials
Raw materials
Preparation Products
1-PHENYL-1H-INDOLE Suppliers
- Tel
- 03-36680489
- Fax
- 03-3668-0520
- Sales-JP@TCIchemicals.com
- Country
- Japan
- ProdList
- 28387
- Advantage
- 80
View Lastest Price from 1-PHENYL-1H-INDOLE manufacturers
- Product
- 1-Phenylindole 16096-33-6
- Price
- US $2600.00/g
- Min. Order
- 1g
- Purity
- 99
- Supply Ability
- 500 Kg
- Release date
- 2024-11-18
- Product
- 1-PHENYL-1H-INDOLE 16096-33-6
- Price
- US $8.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10tons
- Release date
- 2018-12-24