3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE
- Product Name
- 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE
- CAS No.
- 39741-46-3
- Chemical Name
- 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE
- Synonyms
- 5-Bromo-3-(chloromethyl)pyridine hydrochloride;3-Bromo-5-(chloromethyl)pyridine hydrochloride 95%;3-Bromo-5-(chloromethyl)pyridine hydrochloride 95+%;3-bromo-5-(chloromethyl)-Pyridine hydrochloride (1:1);Pyridine, 3-bromo-5-(chloromethyl)-, hydrochloride (1:1)
- CBNumber
- CB21010330
- Molecular Formula
- C6H5BrClN.ClH
- Formula Weight
- 0
- MOL File
- 39741-46-3.mol
3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE Property
- storage temp.
- Inert atmosphere,Room Temperature
- form
- crystalline solid
- color
- White to off-white
- CAS DataBase Reference
- 39741-46-3
Safety
- Hazard Codes
- C
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H314Causes severe skin burns and eye damage
H318Causes serious eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- B415535
- Product name
- 3-Bromo-5-(chloromethyl)pyridineHydrochloride
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- V1765
- Product name
- 3-Bromo-5-(chloromethyl)pyridinehydrochloride
- Packaging
- 250mg
- Price
- $64
- Updated
- 2021/12/16
- Product number
- OR14923
- Product name
- 3-Bromo-5-(chloromethyl)pyridinehydrochloride
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $174
- Updated
- 2021/12/16
- Product number
- 3H32-D-60
- Product name
- 3-Bromo-5-(chloromethyl)pyridinehydrochloride
- Purity
- 95%
- Packaging
- 250mg
- Price
- $192
- Updated
- 2021/12/16
- Product number
- OR14923
- Product name
- 3-Bromo-5-(chloromethyl)pyridinehydrochloride
- Purity
- 95+%
- Packaging
- 1g
- Price
- $290
- Updated
- 2021/12/16
3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE Chemical Properties,Usage,Production
Synthesis
37669-64-0
39741-46-3
The general procedure for the synthesis of 3-bromo-5-(chloromethyl)pyridine hydrochloride from 3-bromopyridine-5-methanol was as follows: (5-bromopyridin-3-yl)methanol (XLV) (1.54 g, 8.2 mmol) was dissolved in a dioxane solution (10 mL) of 4 M HCl at 0 °C, followed by evaporation treatment. The resulting residue was dissolved in SOCl2 (4 mL) and reacted under reflux conditions for 2 hours. Upon completion of the reaction, SOCl2 was removed and the residue was ground with hexane to afford the HCl salt of 3-bromo-5-(chloromethyl)pyridine (XLVT) as a brown solid (1.30 g, 5.4 mmol, 66% yield). The product was used for subsequent experiments without further purification.ESIMS analysis showed that the product C6H5BrClN had a m/z of 206 (M + H).
References
[1] Patent: WO2013/40215, 2013, A1. Location in patent: Paragraph 00268
[2] Nucleosides and Nucleotides, 1994, vol. 13, # 10, p. 2345 - 2366
[3] Patent: WO2012/148808, 2012, A1. Location in patent: Page/Page column 78
[4] Patent: WO2018/75858, 2018, A1. Location in patent: Paragraph 0299; 0301
3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE Preparation Products And Raw materials
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View Lastest Price from 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE manufacturers
- Product
- 3-Bromo-5-(chloromethyl)pyridine hydrochloride 39741-46-3
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000 tons
- Release date
- 2019-12-30
- Product
- 3-BROMO-5-(CHLOROMETHYL)PYRIDINE HYDROCHLORIDE 39741-46-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 100kg
- Release date
- 2020-01-18