3-OXO-3-(3-PYRIDINYL)PROPANENITRILE
- Product Name
- 3-OXO-3-(3-PYRIDINYL)PROPANENITRILE
- CAS No.
- 30510-18-0
- Chemical Name
- 3-OXO-3-(3-PYRIDINYL)PROPANENITRILE
- Synonyms
- b-oxo-3-Pyridinepropanenitrile;3-Pyridinepropanenitrile, β-oxo-;Beta-oxo-3-Pyridinepropanenitrile;3-Oxo-3-(3-pyridyl)propanenitrile;3-OXO-3-PYRIDIN-3-YL-PROPIONITRILE;3-Oxo-3-pyridin-3-ylpropanenitrile;3-OXO-3-(3-PYRIDINYL)PROPANENITRILE;3-oxo-3-(yridine-3-yl)propanenitrile;3-oxo-3-(pyridine-3-yl)propanenitrile;3-Pyridinepropanenitrile, .beta.-oxo-
- CBNumber
- CB2103554
- Molecular Formula
- C8H6N2O
- Formula Weight
- 146.15
- MOL File
- 30510-18-0.mol
3-OXO-3-(3-PYRIDINYL)PROPANENITRILE Property
- Melting point:
- 79-81°C
- Boiling point:
- 344.3±22.0 °C(Predicted)
- Density
- 1.177±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- form
- solid
- pka
- 6.46±0.10(Predicted)
- color
- Orange
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- O990063
- Product name
- 3-Oxo-3-pyridin-3-ylPropionitrile
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- O990063
- Product name
- 3-Oxo-3-pyridin-3-ylPropionitrile
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- 046707
- Product name
- 3-Oxo-3-(3-pyridinyl)propanenitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $91
- Updated
- 2021/12/16
- Product number
- 4H37-1-P8
- Product name
- 3-Oxo-3-pyridin-3-ylpropanenitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $93
- Updated
- 2021/12/16
- Product number
- 046707
- Product name
- 3-Oxo-3-(3-pyridinyl)propanenitrile
- Purity
- 97%
- Packaging
- 5g
- Price
- $260
- Updated
- 2021/12/16
3-OXO-3-(3-PYRIDINYL)PROPANENITRILE Chemical Properties,Usage,Production
Synthesis
93-60-7
75-05-8
30510-18-0
To a stirred solution of methyl nicotinate (XVIII; 8 g; 58 mmol) in toluene (110 mL) at 0 °C was slowly added sodium hydride (2.8 g; 110 mmol). The reaction mixture was kept stirred at 0 °C for 30 min, followed by dropwise addition of acetonitrile (12 g; 91 mmol). The reaction mixture was heated to reflux for 72 hours. After completion of the reaction, the mixture was cooled, concentrated under reduced pressure and diluted with ice-cold water. The pH of the reaction mixture was adjusted to acidic with glacial acetic acid. Subsequently, the aqueous layer was extracted with ethyl acetate (3 x 100 mL). The organic layers were combined, washed with saturated brine, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 3-oxo-3-(pyridin-3-yl)propanenitrile (XIX; 6 g, 70% yield) as a yellow solid. Mass spectrometry analysis showed [M-1]? peak at 145.01.
References
[1] Patent: WO2015/97122, 2015, A1. Location in patent: Page/Page column 81; 82
[2] Patent: WO2012/129258, 2012, A1. Location in patent: Page/Page column 150; 151
3-OXO-3-(3-PYRIDINYL)PROPANENITRILE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-OXO-3-(3-PYRIDINYL)PROPANENITRILE manufacturers
- Product
- 3-OXO-3-(3-PYRIDINYL)PROPANENITRILE 30510-18-0
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-27
- Product
- 3-OXO-3-(3-PYRIDINYL)PROPANENITRILE 30510-18-0
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG
- Release date
- 2019-07-09
- Product
- 3-OXO-3-(3-PYRIDINYL)PROPANENITRILE 30510-18-0
- Price
- US $1.00/Kg
- Min. Order
- 1Kg/Bag
- Purity
- 99.95
- Supply Ability
- 500kg
- Release date
- 2019-04-15