ChemicalBook > CAS DataBase List > Phenol, 3-fluoro-5-methyl- (9CI)

Phenol, 3-fluoro-5-methyl- (9CI)

Product Name
Phenol, 3-fluoro-5-methyl- (9CI)
CAS No.
216976-31-7
Chemical Name
Phenol, 3-fluoro-5-methyl- (9CI)
Synonyms
3-Fluoro-5-hydroxytoluene;Phenol, 3-fluoro-5-methyl-;3-Fluoro-5-methylphenol97%;3-Fluoro-5-methylphenol 97%;Phenol, 3-fluoro-5-methyl- (9CI);3-Fluoro-5-hydroxytoluene, 5-Fluoro-m-cresol
CBNumber
CB21072635
Molecular Formula
C7H7FO
Formula Weight
126.13
MOL File
216976-31-7.mol
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Phenol, 3-fluoro-5-methyl- (9CI) Property

Boiling point:
199.8±20.0 °C(Predicted)
Density 
1.164±0.06 g/cm3(Predicted)
storage temp. 
2-8°C
pka
9.08±0.10(Predicted)
Appearance
Light yellow to yellow Liquid
CAS DataBase Reference
216976-31-7
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Safety

Hazard Codes 
T
HazardClass 
8
HS Code 
2908990000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H227Combustible liquid

H302Harmful if swallowed

H312Harmful in contact with skin

H314Causes severe skin burns and eye damage

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P309IF exposed or if you feel unwell:

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC
Product number
F597148
Product name
3-Fluoro-5-methylphenol
Packaging
250mg
Price
$55
Updated
2021/12/16
SynQuest Laboratories
Product number
2701-3-08
Product name
3-Fluoro-5-methylphenol
Purity
98%
Packaging
5G
Price
$111
Updated
2021/12/16
Matrix Scientific
Product number
116612
Product name
3-Fluoro-5-methylphenol
Packaging
5g
Price
$221
Updated
2021/12/16
SynQuest Laboratories
Product number
2701-3-08
Product name
3-Fluoro-5-methylphenol
Purity
98%
Packaging
25g
Price
$306
Updated
2021/12/16
Matrix Scientific
Product number
116612
Product name
3-Fluoro-5-methylphenol
Packaging
10g
Price
$406
Updated
2021/12/16
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Phenol, 3-fluoro-5-methyl- (9CI) Chemical Properties,Usage,Production

Synthesis

160911-11-5

216976-31-7

General procedure for the synthesis of 3-fluoro-5-methylphenol from 1-fluoro-3-methoxy-5-methylbenzene: (40b) Synthesis of 1-fluoro-5-methylphenol In Example (40a), 1-fluoro-3-methoxy-5-methylbenzene (0.92 g, 6.56 mmol) was dissolved in dichloromethane (20 mL), boron tribromide (1.0 M solution in dichloromethane, 8.53 mL, 8.53 mmol) was added, and the reaction was stirred for 10 hours at 0°C. After completion of the reaction, water (100 mL) was added to the reaction mixture and extracted with dichloromethane (100 mL). The organic layers were combined and dried over anhydrous sodium sulfate. After concentration under reduced pressure, the residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate, 1:1) to afford 3-fluoro-5-methylphenol (0.83 g, yield: 99%) as a yellow oil. 1H-NMR (CDCl3, 400 MHz) δ: 2.06 (3H, s), 4.97 (1H, s), 6.37 (1H, dt, J = 2.4, 10.2 Hz), 6.44 (1H, s), 6.48 (1H, d, J = 8.6 Hz).

References

[1] Patent: EP2138484, 2009, A1. Location in patent: Page/Page column 44

Phenol, 3-fluoro-5-methyl- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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216976-31-7, Phenol, 3-fluoro-5-methyl- (9CI)Related Search:

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  • Phenol, 3-fluoro-5-methyl- (9CI)
  • 3-Fluoro-5-hydroxytoluene, 5-Fluoro-m-cresol
  • 3-Fluoro-5-methylphenol97%
  • 3-Fluoro-5-methylphenol 97%
  • 3-Fluoro-5-hydroxytoluene
  • Phenol, 3-fluoro-5-methyl-
  • 216976-31-7
  • HALIDE
  • ALCOHOL