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Dicyclohexylborane

Product Name
Dicyclohexylborane
CAS No.
1568-65-6
Chemical Name
Dicyclohexylborane
Synonyms
icyclohexylboron;Dicyclohexylborane;Borane, dicyclohexyl-
CBNumber
CB21074659
Molecular Formula
C12H23B
Formula Weight
178.12
MOL File
1568-65-6.mol
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Dicyclohexylborane Property

Melting point:
103-105 °C
Boiling point:
263.7±23.0 °C(Predicted)
solubility 
Soluble in THF, diethyl ether, dichloromethane, and pentane.
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Safety

Hazard Codes 
F,C
Risk Statements 
17-34
Safety Statements 
16-23-26-36/37/39-45
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H250Catches fire spontaneously if exposed to air

H314Causes severe skin burns and eye damage

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P222Do not allow contact with air.

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P330+P331IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.

P302+P334IF ON SKIN: Immerse in cool water/wrap in wet bandages.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P363Wash contaminated clothing before reuse.

P370+P378In case of fire: Use … for extinction.

P405Store locked up.

P422Store contents under …

P501Dispose of contents/container to..…

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Dicyclohexylborane Chemical Properties,Usage,Production

Uses

Dicyclohexylborane is a reducing reagent such as in the synthesis of chlorosulfolipid products such as deschloromytilipin A.

Synthesis Reference(s)

Journal of the American Chemical Society, 95, p. 6876, 1973 DOI: 10.1021/ja00801a081

Reactivity Profile

Dicyclohexylborane is a reagent for the reduction of ketones and α,β-unsaturated ketones; it is used for the hydroboration of alkynes, alkenes, and allenes.

Synthesis

Dicyclohexylborane is a stable white solid available via the hydroboration of cyclohexene with either Borane-Tetrahydrofuran or Borane-Dimethyl Sulfide. Recently, dicyclohexylborane has been prepared via the hydroboration of cyclohexene with borane-1,4-thioxane.

Precautions

Dicyclohexylborane must be used immediately upon generation or stored as a solid under dry nitrogen. Use in a fume hood.

Dicyclohexylborane Preparation Products And Raw materials

Raw materials

Preparation Products

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Dicyclohexylborane Suppliers

TIANJIN SPRING PHARMA SCIENCE CO., LTD.
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Hunan HuaTeng Pharmaceutical Co., Ltd.,
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ShangHai Siyan Biological Technology Co., Ltd.
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parabiochem
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Nanjing NingFan Pharm-Tech CO. LTD.
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Zhengzhou Acme Chemical Co., Ltd.
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Hefei TNJ Chemical Industry Co.,Ltd.
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Dayang Chem (Hangzhou) Co.,Ltd.
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AFINE CHEMICALS LIMITED
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View Lastest Price from Dicyclohexylborane manufacturers

Career Henan Chemical Co
Product
Dicyclohexylborane 1568-65-6
Price
US $1.00/ASSAYS
Min. Order
1ASSAYS
Purity
99.99%
Supply Ability
200kg
Release date
2019-12-20

1568-65-6, DicyclohexylboraneRelated Search:


  • Dicyclohexylborane
  • Borane, dicyclohexyl-
  • icyclohexylboron
  • 1568-65-6