3-(3-Hydroxyphenyl)benzoic acid

Product Name: 3-(3-Hydroxyphenyl)benzoic acid
CAS No.: 171047-01-1
Chemical Name: 3-(3-Hydroxyphenyl)benzoic acid
Synonyms: 3-(3-Hydroxyphenyl)benzoic acid;3'-Hydroxy-[1,1'-biphenyl]-3-carboxylic acid;[1,1'-Biphenyl]-3-carboxylic acid, 3'-hydroxy-;3′-Hydroxy-biphenyl-3-carboxylic acid, CAS 171047-01-1
CBNumber: CB21455232
Molecular Formula: C13H10O3
Formula Weight: 214.22
MOL File: 171047-01-1.mol

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3-(3-Hydroxyphenyl)benzoic acid Property

storage temp.: Sealed in dry,Room Temperature

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: H817623
Product name: 3''-Hydroxy-biphenyl-3-carboxylicAcid
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: H817623
Product name: 3''-Hydroxy-biphenyl-3-carboxylicAcid
Packaging: 500mg
Price: $285
Updated: 2021/12/16

AK Scientific

Product number: 8793AA
Product name: 3'-Hydroxy-[1,1'-biphenyl]-3-carboxylicacid
Packaging: 250mg
Price: $137
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0092567
Product name: 3'-HYDROXY-BIPHENYL-3-CARBOXYLIC ACID
Purity: 95.00%
Packaging: 1G
Price: $1280.66
Updated: 2021/12/16

Ambeed

Product number: A378365
Product name: 3'-Hydroxy-[1,1'-biphenyl]-3-carboxylicacid
Purity: 97%
Packaging: 250mg
Price: $93
Updated: 2021/12/16

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3-(3-Hydroxyphenyl)benzoic acid Chemical Properties,Usage,Production

Synthesis

585-76-2

87199-18-6

171047-01-1

General method: m-Bromobenzoic acid (1.0 eq.) was dissolved in a solvent mixture of water and dioxane (1:1). 3-Hydroxyphenylboronic acid (1.5 eq.) and potassium phosphate (5.0 eq.) were added. The solution was degassed by vacuum/argon cycles (10 times) and further degassed (5 times) before addition of PdCl2(PPh3)2 (10 mol%). The resulting mixture was stirred at 95 °C and under argon atmosphere for 16-20 hours. Upon completion of the reaction, the reaction mixture was filtered through diatomaceous earth, diluted with water (~30 mL) and then washed with chloroform (3 x 30 mL). The aqueous phase was concentrated under reduced pressure and subsequently purified by a C18 pre-column and further purified on a 10 g or 60 g C18 column using a gradient elution with aqueous acetonitrile (10-100%) to give 3'-hydroxybiphenyl-3-carboxylic acid.

References

[1] European Journal of Medicinal Chemistry, 2018, vol. 145, p. 634 - 648

3-(3-Hydroxyphenyl)benzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(3-Hydroxyphenyl)benzoic acid Suppliers

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3-(3-Hydroxyphenyl)benzoic acid

[1,1'-Biphenyl]-3-carboxylic acid, 3'-hydroxy-

3'-Hydroxy-[1,1'-biphenyl]-3-carboxylic acid

3′-Hydroxy-biphenyl-3-carboxylic acid, CAS 171047-01-1

171047-01-1