ChemicalBook > CAS DataBase List > 3-MORPHOLIN-4-YLMETHYLBENZOIC ACID

3-MORPHOLIN-4-YLMETHYLBENZOIC ACID

Product Name: 3-MORPHOLIN-4-YLMETHYLBENZOIC ACID
CAS No.: 67451-81-4
Chemical Name: 3-MORPHOLIN-4-YLMETHYLBENZOIC ACID
Synonyms: AKOS BB-9413;3-(Morpholinomethyl);3-(Morpholinomethyl)benzoic Acid;3-MORPHOLIN-4-YLMETHYLBENZOIC ACID;3-(4-Morpholinylmethyl)Benzoic acid;3-Morpholin-4-ylmethylbenzoicacid95%;Benzoic acid, 3-(4-morpholinylmethyl)-;3-MORPHOLIN-4-YLMETHYLBENZOIC ACID 95%
CBNumber: CB2145934
Molecular Formula: C12H15NO3
Formula Weight: 221.25
MOL File: 67451-81-4.mol

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3-MORPHOLIN-4-YLMETHYLBENZOIC ACID Property

Boiling point:: 376.9±32.0 °C(Predicted)
Density: 1.233±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 3.98±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xn
Risk Statements: 22

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: M732740
Product name: 3-(Morpholinomethyl)benzoicAcid
Packaging: 500mg
Price: $155
Updated: 2021/12/16

Matrix Scientific

Product number: 071860
Product name: 3-Morpholin-4-ylmethylbenzoic acid
Purity: 95+%
Packaging: 1g
Price: $347
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: COR0002485
Product name: 3-MORPHOLIN-4-YLMETHYLBENZOIC ACID
Purity: 95.00%
Packaging: 1G
Price: $258.3
Updated: 2021/12/16

Matrix Scientific

Product number: 071860
Product name: 3-Morpholin-4-ylmethylbenzoic acid
Purity: 95+%
Packaging: 5g
Price: $998
Updated: 2021/12/16

Matrix Scientific

Product number: 071860
Product name: 3-Morpholin-4-ylmethylbenzoic acid
Purity: 95+%
Packaging: 10g
Price: $1519
Updated: 2021/12/16

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3-MORPHOLIN-4-YLMETHYLBENZOIC ACID Chemical Properties,Usage,Production

Synthesis

190660-95-8

67451-81-4

General procedure for the synthesis of 3-morpholin-4-ylmethylbenzoic acid from methyl 3-(4-morpholinylmethyl)benzoate: to a solution of methyl 3-(4-morpholinylmethyl)benzoate (5.02 g, 21.0 mmol) in methanol (100 mL) was added a sodium hydroxide solution (21.0 mL, 42.0 mmol, 2M). The reaction mixture was heated at 50 °C with stirring for 16 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The residue was adjusted to pH=3 with 1M hydrochloric acid and the resulting suspension was subsequently filtered. The collected solid was dissolved in acetonitrile (15 mL) and concentrated to afford 3-(morpholin-4-ylmethyl)benzoic acid (4.6 g, 100% yield) as a white solid, which was used directly in the subsequent reaction without further purification.

References

[1] Patent: WO2018/169777, 2018, A1. Location in patent: Paragraph 0229

3-MORPHOLIN-4-YLMETHYLBENZOIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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3-MORPHOLIN-4-YLMETHYLBENZOIC ACID Suppliers

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3-MORPHOLIN-4-YLMETHYLBENZOIC ACID

AKOS BB-9413

3-Morpholin-4-ylmethylbenzoicacid95%

3-MORPHOLIN-4-YLMETHYLBENZOIC ACID 95%

3-(4-Morpholinylmethyl)Benzoic acid

3-(Morpholinomethyl)

3-(Morpholinomethyl)benzoic Acid

Benzoic acid, 3-(4-morpholinylmethyl)-

67451-81-4