ChemicalBook > CAS DataBase List > 3-Amino-2-iodo-6-(trifluoromethyl)-pyridine

3-Amino-2-iodo-6-(trifluoromethyl)-pyridine

Product Name
3-Amino-2-iodo-6-(trifluoromethyl)-pyridine
CAS No.
920979-04-0
Chemical Name
3-Amino-2-iodo-6-(trifluoromethyl)-pyridine
Synonyms
124947;3-Amino-6-iodo-2-trifluoromethylpyridine;5-Amino-6-iodo-2-(trifluoromethyl)pyridine;2-IODO-6-TRIFLUOROMETHYL-PYRIDIN-3-YLAMINE;3-Amino-2-iodo-6-(trifluoromethyl)-pyridine;3-Pyridinamine, 2-iodo-6-(trifluoromethyl)-;2-IODO-6-( TRIFLUOROMETHYL) PYRIDINE-3- AMINE
CBNumber
CB21471179
Molecular Formula
C6H4F3IN2
Formula Weight
288.01
MOL File
920979-04-0.mol
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3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Property

storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
Appearance
White to off-white Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific
Product number
PC446152
Product name
2-Iodo-6-(trifluoromethyl)pyridin-3-ylamine
Purity
95+%
Packaging
1g
Price
$356
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0363905
Product name
2-IODO-6-(TRIFLUOROMETHYL)PYRIDIN-3-AMINE
Purity
95.00%
Packaging
5MG
Price
$500.76
Updated
2021/12/16
SynQuest Laboratories
Product number
3H30-K-02
Product name
2-Iodo-6-(trifluoromethyl)pyridin-3-ylamine
Purity
95.0%
Packaging
1g
Price
$570
Updated
2021/12/16
AK Scientific
Product number
5557AC
Product name
2-Iodo-6-(trifluoromethyl)pyridin-3-amine
Packaging
10g
Price
$1339
Updated
2021/12/16
Alichem
Product number
920979040
Product name
3-Amino-2-iodo-6-(trifluoromethyl)pyridine
Packaging
5g
Price
$1594.73
Updated
2021/12/16
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3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Chemical Properties,Usage,Production

Synthesis

106877-33-2

920979-04-0

General procedure for the preparation of Example IV 3-amino-2-iodo-6-(trifluoromethyl)pyridine: 3.85 g (12.3 mmol) of silver sulfate was added to a 100 mL ethanol solution containing 2 g (12.3 mmol) of 5-amino-2-(trifluoromethyl)pyridine under stirring and room temperature conditions. Subsequently, 3.13 g of iodine was added to the reaction system and stirred continuously for 24 hours at room temperature. Upon completion of the reaction, the suspended solids in the reaction medium were removed by filtration and the filtrate was concentrated under reduced pressure. The concentrated residue was dissolved in 200 mL of dichloromethane, washed sequentially with 5% sodium hydroxide solution and water, and the organic phase was dried with magnesium sulfate. Finally, the dried organic phase was concentrated under reduced pressure to afford 3.42 g of the target product 3-amino-2-iodo-6-(trifluoromethyl)pyridine as a pink solid in 96% yield and with a melting point of 127 °C.

References

[1] Patent: US2008/200495, 2008, A1. Location in patent: Page/Page column 6
[2] Patent: US2008/125459, 2008, A1. Location in patent: Page/Page column 16
[3] Patent: US2009/42873, 2009, A1. Location in patent: Page/Page column 25
[4] Patent: US2010/41634, 2010, A1. Location in patent: Page/Page column 19-20
[5] Patent: WO2010/91310, 2010, A1. Location in patent: Page/Page column 142

3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Amino-2-iodo-6-(trifluoromethyl)-pyridine Suppliers

China 37 Germany 1 India 1 United States 6 Global 45
Alchem Pharmtech,Inc.
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Matrix Scientific
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920979-04-0, 3-Amino-2-iodo-6-(trifluoromethyl)-pyridineRelated Search:

2-TRIFLUOROMETHYL-3-AMINOPYRIDINE 2-IODO-PYRIDIN-3-YLAMINE 5-AMINO-2-IODOPYRIDINE 5-Amino-2-(trifluoromethyl)pyridine 2-Iodo-6-methylpyridine 3-Amino-2-iodo-6-(trifluoromethyl)-pyridine

  • 3-Amino-2-iodo-6-(trifluoromethyl)-pyridine
  • 3-Amino-6-iodo-2-trifluoromethylpyridine
  • 2-IODO-6-TRIFLUOROMETHYL-PYRIDIN-3-YLAMINE
  • 5-Amino-6-iodo-2-(trifluoromethyl)pyridine
  • 2-IODO-6-( TRIFLUOROMETHYL) PYRIDINE-3- AMINE
  • 124947
  • 3-Pyridinamine, 2-iodo-6-(trifluoromethyl)-
  • 920979-04-0
  • C6H4F3IN2