ChemicalBook > CAS DataBase List > 8-BROMO-5-NITROQUINOLINE

8-BROMO-5-NITROQUINOLINE

Product Name: 8-BROMO-5-NITROQUINOLINE
CAS No.: 139366-35-1
Chemical Name: 8-BROMO-5-NITROQUINOLINE
Synonyms: 8-BROMO-5-NITROQUINOLINE;Quinoline, 8-bromo-5-nitro-
CBNumber: CB21479953
Molecular Formula: C9H5BrN2O2
Formula Weight: 253.05
MOL File: 139366-35-1.mol

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8-BROMO-5-NITROQUINOLINE Property

Melting point:: 136-137 °C
Boiling point:: 370.5±27.0 °C(Predicted)
Density: 1.747±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 0.16±0.29(Predicted)
Appearance: Light yellow to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B698060
Product name: 8-Bromo-5-nitroquinoline
Packaging: 1g
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB150928
Product name: 8-Bromo-5-nitroquinoline
Packaging: 100mg
Price: $76
Updated: 2021/12/16

AK Scientific

Product number: V2973
Product name: 8-Bromo-5-nitroquinoline
Packaging: 1g
Price: $107
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB150928
Product name: 8-Bromo-5-nitroquinoline
Packaging: 250mg
Price: $150
Updated: 2021/12/16

Matrix Scientific

Product number: 136731
Product name: 8-Bromo-5-nitroquinoline
Purity: 95%+
Packaging: 1g
Price: $208
Updated: 2021/12/16

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8-BROMO-5-NITROQUINOLINE Chemical Properties,Usage,Production

Synthesis

16567-18-3

139366-35-1

A. Synthesis of 8-bromo-5-nitroquinoline (464A): 8-bromoquinoline (25.00 g, 120.2 mmol) was dissolved in concentrated sulfuric acid (82.5 mL) at room temperature, and the reaction system was subsequently cooled to 0°C. Fuming nitric acid (32.5 mL) was slowly added dropwise over 10 minutes. After the dropwise addition was completed, the reaction system was gradually warmed to room temperature, followed by further heating to 65 °C. After 48 hours of continuous reaction at 65 °C, the reaction mixture was cooled to room temperature and slowly poured into ice (500 g). The mixture was extracted with dichloromethane (5 x 200 mL). The organic layers were combined, washed once with saturated brine and dried over anhydrous sodium sulfate. The organic phase was concentrated under reduced pressure to give the crude product 464A as a light yellow solid (28.6 g, 94% yield).HPLC analysis: purity 98%, retention time 2.717 min (YMC S5 ODS column, 4.6 × 50 mm, mobile phase 10-90% aqueous methanol containing 0.2% phosphoric acid, gradient elution 4 min, flow rate 4 mL/min, detection wavelength (220 nm).

References

[1] Patent: US2004/77605, 2004, A1
[2] Patent: US2005/119228, 2005, A1
[3] Organic and Biomolecular Chemistry, 2016, vol. 14, # 6, p. 1969 - 1981
[4] Recueil des Travaux Chimiques des Pays-Bas, 1929, vol. 48, p. 552
[5] Journal fuer Praktische Chemie (Leipzig), 1893, vol. <2> 48, p. 158

8-BROMO-5-NITROQUINOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 8-BROMO-5-NITROQUINOLINE manufacturers

Shanghai Rlavie Technology Co ltd

Product: 8-Bromo-5-nitroquinoline 139366-35-1
Price: US $0.00-0.00/kg
Min. Order: 0.0001kg
Purity: 98%min
Supply Ability: 100kgs/month
Release date: 2022-05-09

Career Henan Chemical Co

Product: 8-BROMO-5-NITROQUINOLINE 139366-35-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 97%-99.9%
Supply Ability: 200kg
Release date: 2020-03-05

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