2-FLUORO-4-NITROBENZONITRILE

Product Name: 2-FLUORO-4-NITROBENZONITRILE
CAS No.: 34667-88-4
Chemical Name: 2-FLUORO-4-NITROBENZONITRILE
Synonyms: 2-FLUORO-4-NITROBENZONITRILE;2-Fluoro-4-nitrobenzonitrile ,98%;Benzonitrile, 2- fluoro- 4- nitro-
CBNumber: CB2166124
Molecular Formula: C7H3FN2O2
Formula Weight: 166.11
MOL File: 34667-88-4.mol

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2-FLUORO-4-NITROBENZONITRILE Property

Melting point:: 0°C
Boiling point:: 0°C
Density: 1.41±0.1 g/cm3(Predicted)
Flash point:: 0°C
storage temp.: Sealed in dry,Room Temperature
Appearance: Off-white to light yellow Solid
CAS DataBase Reference: 34667-88-4(CAS DataBase Reference)

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Safety

Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39-36
RIDADR: 3439
HS Code: 29269090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: F595063
Product name: 2-Fluoro-4-nitrobenzonitrile
Packaging: 1g
Price: $55
Updated: 2021/12/16

Matrix Scientific

Product number: 119104
Product name: 2-Fluoro-4-nitrobenzonitrile
Purity: 95+%
Packaging: 1g
Price: $98
Updated: 2021/12/16

Frontier Specialty Chemicals

Product number: JK297891
Product name: 2-Fluoro-4-nitrobenzonitrile
Purity: 98%
Packaging: 5g
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: F228
Product name: 2-Fluoro-4-nitro-benzonitrile
Packaging: 25g
Price: $114
Updated: 2021/12/16

Apolloscientific

Product number: PC502594
Product name: 2-Fluoro-4-nitrobenzonitrile
Packaging: 25g
Price: $160
Updated: 2021/12/16

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2-FLUORO-4-NITROBENZONITRILE Chemical Properties,Usage,Production

Chemical Properties

Light yellow solid

Synthesis

350-32-3

34667-88-4

General procedure for the synthesis of 2-fluoro-4-nitrobenzonitrile from 2-fluoro-4-nitrobenzamide: A mixture of 2-fluoro-4-nitrobenzamide (0.83 g, 4.6 mmol) and phosphorus pentoxide/hexamethyldisiloxane in 1,2-dichloroethane (20 mL) was heated and refluxed for 4 hr at 100 °C under nitrogen atmosphere. Upon completion of the reaction, the mixture was cooled to room temperature and subsequently filtered through a silicone plug, washed first with hexane (200 mL) and then with 5% methanol/chloroform mixture (400 mL). The methanol/chloroform washings were combined and concentrated under reduced pressure to give 2-fluoro-4-nitrobenzonitrile (0.71 g, 95% yield) as a beige solid.1H NMR (DMSO-d6) data were as follows: δ 8.46 (dd, J = 9.5, 2.0 Hz, 1H), 8.37-8.22 (m, 2H).

References

[1] Journal of Heterocyclic Chemistry, 1997, vol. 34, # 4, p. 1163 - 1172
[2] Patent: US6344459, 2002, B1. Location in patent: Page column 70-71
[3] European Journal of Medicinal Chemistry, 2018, vol. 143, p. 1325 - 1344
[4] Journal of Medicinal Chemistry, 2001, vol. 44, # 23, p. 3856 - 3871

2-FLUORO-4-NITROBENZONITRILE Preparation Products And Raw materials

Raw materials

Ethanol Potassium carbonate Chromium(VI) oxide Triethylamine Tetrahydrofuran Trifluoroacetic anhydride Diethyl ether Ethyl acetate Oxalyl chloride 2-Fluoro-4-nitrotoluene Sulfuric acid

Preparation Products

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2-FLUORO-4-NITROBENZONITRILE Suppliers

China 109 Europe 2 Germany 2 India 2 Ukraine 1 United Kingdom 6 United States 17 Global 139

J & K SCIENTIFIC LTD.

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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

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View Lastest Price from 2-FLUORO-4-NITROBENZONITRILE manufacturers

Career Henan Chemical Co

Product: 2-FLUORO-4-NITROBENZONITRILE 34667-88-4
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-11

34667-88-4, 2-FLUORO-4-NITROBENZONITRILERelated Search:

2-AMINO-5-FLUORO-4-NITROBENZONITRILE 3-Fluoro-2-nitrobenzonitrile 3-FLUORO-5-NITROBENZONITRILE, 97% MIN.,3-FLUORO-5-NITROBENZONITRILE 2-FLUORO-5-NITROBENZONITRILE,2-Fluoro-5-nitrobenzonitrile, 98+%,2-Fluoro-5-nitrobenzonitrile97%,2-Fluoro-5-nitrobenzonitrile 97% 2-FLUORO-6-NITROBENZONITRILE 2-CHLORO-6-FLUORO-3-NITROBENZONITRILE 3-FLUORO-4-NITROBENZONITRILE 4-FLUORO-2-NITROBENZONITRILE 2-bromo-4-fluoro-5-nitrobenzonitrile 4-amino-2-fluoro-5-nitrobenzonitrile 5-FLUORO-2-NITROBENZONITRILE,5-Fluoro-2-nitrobenzonitrile 98%,5-Fluoro-2-nitrobenzonitrile98% 4-FLUORO-3-NITROBENZONITRILE 2-Fluoro-4-nitrotoluene 4-Nitrobenzonitrile 4-AMINO-2-FLUOROBENZONITRILE 2-FLUORO-4-NITROBENZONITRILE

2-FLUORO-4-NITROBENZONITRILE

Benzonitrile, 2- fluoro- 4- nitro-

2-Fluoro-4-nitrobenzonitrile ,98%

34667-88-4

207979-19-4

C7H3N2O2F

Fluorine series