5-Thiazolecarboxaldehyde, 2-cyclopropyl-

Product Name: 5-Thiazolecarboxaldehyde, 2-cyclopropyl-
CAS No.: 877385-86-9
Chemical Name: 5-Thiazolecarboxaldehyde, 2-cyclopropyl-
Synonyms: 2-Cyclopropyl-5-formyl-1,3-thiazole;2-cyclopropylthiazole-5-carbaldehyde;2-cyclopropyl-5-Thiazolecarboxaldehyde;5-Thiazolecarboxaldehyde, 2-cyclopropyl-;2-Cyclopropyl-1,3-thiazole-5-carboxaldehyde
CBNumber: CB21863530
Molecular Formula: C7H7NOS
Formula Weight: 153.2
MOL File: 877385-86-9.mol

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5-Thiazolecarboxaldehyde, 2-cyclopropyl- Property

Boiling point:: 278.5±13.0 °C(Predicted)
Density: 1.370±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 1.66±0.10(Predicted)
Appearance: Light yellow to yellow Solid
InChI: InChI=1S/C7H7NOS/c9-4-6-3-8-7(10-6)5-1-2-5/h3-5H,1-2H2
InChIKey: ORNIFVGIJQCIMW-UHFFFAOYSA-N
SMILES: S1C(C=O)=CN=C1C1CC1

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Safety

HS Code: 2934100090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: C993273
Product name: 2-Cyclopropylthiazole-5-carbaldehyde
Packaging: 5mg
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC141855
Product name: 2-Cyclopropylthiazole-5-carbaldehyde
Packaging: 50mg
Price: $84
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC141855
Product name: 2-Cyclopropylthiazole-5-carbaldehyde
Packaging: 100mg
Price: $146
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC141855
Product name: 2-Cyclopropylthiazole-5-carbaldehyde
Packaging: 250mg
Price: $292.5
Updated: 2021/12/16

AK Scientific

Product number: Y4445
Product name: 2-Cyclopropylthiazole-5-carbaldehyde
Packaging: 250mg
Price: $388
Updated: 2021/12/16

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5-Thiazolecarboxaldehyde, 2-cyclopropyl- Chemical Properties,Usage,Production

Synthesis

1159821-56-3

68-12-2

877385-86-9

Compound 10b (1.8 g, 14.4 mmol) was dissolved in tetrahydrofuran (30 mL) under nitrogen protection and cooled to -78 °C. 2.5 M n-butyllithium (n-BuLi) solution (6.3 mL, 15.8 mmol) was slowly added dropwise and the reaction mixture was stirred at this temperature for 1 hour. Subsequently, N,N-dimethylformamide (DMF) (1.6 g, 21.6 mmol) was added and the mixture was gradually warmed to room temperature and stirring was continued for 3 hours. After completion of the reaction, the reaction was quenched with saturated ammonium chloride (NH4Cl) solution and extracted with ethyl acetate (EtOAc). The organic layers were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure. Finally, the crude product was purified by silica gel (SiO2) column chromatography with the eluent being a solvent mixture of petroleum ether and ethyl acetate (the ratio was varied from 50:1 to 20:1 gradient) to give the target compound 10c (1.5 g, 49% yield).

References

[1] Patent: WO2014/110705, 2014, A1. Location in patent: Page/Page column 70
[2] Patent: WO2014/110687, 2014, A1. Location in patent: Page/Page column 51
[3] Journal of Medicinal Chemistry, 2017, vol. 60, # 1, p. 290 - 306

5-Thiazolecarboxaldehyde, 2-cyclopropyl- Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-Thiazolecarboxaldehyde, 2-cyclopropyl- manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 2-Cyclopropylthiazole-5-carbaldehyde 877385-86-9
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-09-30

Career Henan Chemical Co

Product: 5-Thiazolecarboxaldehyde, 2-cyclopropyl- 877385-86-9
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2020-02-18

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877385-86-9