3-METHOXY-5-METHYLBENZALDEHYDE
- Product Name
- 3-METHOXY-5-METHYLBENZALDEHYDE
- CAS No.
- 90674-26-3
- Chemical Name
- 3-METHOXY-5-METHYLBENZALDEHYDE
- Synonyms
- 3-METHOXY-5-METHYLBENZALDEHYDE;3-Methoxy-5-hydroxypropiophenone;Benzaldehyde, 3-methoxy-5-methyl-
- CBNumber
- CB22455691
- Molecular Formula
- C9H10O2
- Formula Weight
- 150.17
- MOL File
- 90674-26-3.mol
3-METHOXY-5-METHYLBENZALDEHYDE Property
- Boiling point:
- 85 °C(Press: 2 Torr)
- Density
- 1.062±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2912490090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- M220450
- Product name
- 3-Methoxy-5-methylbenzaldehyde
- Packaging
- 500mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- 116277
- Product name
- 3-Methoxy-5-methylbenzaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $245
- Updated
- 2021/12/16
- Product number
- 5100AC
- Product name
- 3-Methoxy-5-methylbenzaldehyde
- Packaging
- 250mg
- Price
- $96
- Updated
- 2021/12/16
- Product number
- OR938577
- Product name
- 3-Methoxy-5-methylbenzaldehyde
- Purity
- 95%
- Packaging
- 250mg
- Price
- $327
- Updated
- 2021/12/16
- Product number
- 116277
- Product name
- 3-Methoxy-5-methylbenzaldehyde
- Purity
- 97%
- Packaging
- 5g
- Price
- $630
- Updated
- 2021/12/16
3-METHOXY-5-METHYLBENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
119650-44-1
90674-26-3
B) Synthesis of 3-methoxy-5-methylbenzaldehyde: 2-Iodobenzoic acid (4.00 g) was added to a solution of (3-methoxy-5-methylphenyl) methanol (2.20 g) in DMSO (15 mL) at 0 °C and the reaction mixture was stirred. The reaction system was then warmed to room temperature and stirring was continued for 2 hours. Upon completion of the reaction, ethyl acetate (50 mL) and water (10 mL) were added to the mixture and the insoluble material was removed by filtration. The organic phase was separated, washed with saturated brine and dried over anhydrous sodium sulfate. The solvent was removed by concentration under reduced pressure to give the crude product 3-methoxy-5-methylbenzaldehyde (2.00 g) as a yellow oil, which could be used for subsequent reactions without further purification.
References
[1] Journal of the American Chemical Society, 2012, vol. 134, # 30, p. 12402 - 12405
[2] Synthesis, 2007, # 1, p. 65 - 74
[3] Tetrahedron Letters, 1996, vol. 37, # 49, p. 8953 - 8956
[4] European Journal of Organic Chemistry, 2001, # 1, p. 163 - 171
[5] Journal of the American Chemical Society, 2011, vol. 133, # 39, p. 15686 - 15696
3-METHOXY-5-METHYLBENZALDEHYDE Preparation Products And Raw materials
Raw materials
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